Technology Process of C30H48N8O7S
There total 8 articles about C30H48N8O7S which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
chlorotriisopropylsilane; trifluoroacetic acid;
In
dichloromethane;
at 20 ℃;
for 0.5h;
DOI:10.1021/jacs.1c01234
- Guidance literature:
-
With
trifluoroacetic acid;
In
water; acetonitrile;
at 20 ℃;
for 18h;
DOI:10.1126/science.1229753
- Guidance literature:
-
Multi-step reaction with 6 steps
1: triphenylmethyl alcohol / dichloromethane / 2 h / 20 °C
2: benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / dichloromethane / 16 h / 20 °C
3: triphenylmethyl alcohol / dichloromethane / 2 h / 20 °C
4: benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / dichloromethane / 16 h / 20 °C
5: hydrazine hydrate / ethanol; water / 16 h / 20 °C
6: trifluoroacetic acid; chlorotriisopropylsilane / dichloromethane / 0.5 h / 20 °C
With
triphenylmethyl alcohol; hydrazine hydrate; chlorotriisopropylsilane; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; trifluoroacetic acid;
In
ethanol; dichloromethane; water;
DOI:10.1021/jacs.1c01234