C₅₃H₅₉ClF₄N₆O₇S₄

Base Information

Chemical Name:C₅₃H₅₉ClF₄N₆O₇S₄
CAS No.:1391107-89-3
Molecular Formula:C₅₃H₅₉ClF₄N₆O₇S₄
Molecular Weight:1131.8
Hs Code.:

C<sub>53</sub>H<sub>59</sub>ClF<sub>4</sub>N<sub>6</sub>O<sub>7</sub>S<sub>4</sub>

Synonyms:C₅₃H₅₉ClF₄N₆O₇S₄

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₅₃H₅₉ClF₄N₆O₇S₄

Chemical Property:

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Technology Process of C₅₃H₅₉ClF₄N₆O₇S₄

There total 17 articles about C₅₃H₅₉ClF₄N₆O₇S₄ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.0%

: 1402141-79-0
(R)-1-(3-amino-4-(phenylthio)butyl)piperidin-4-ol

: 1619923-53-3
N-(4-(4-(3-(2-(4-chlorophenyl)-1-isopropyl-5-methyl-4-(methylsulfonyl)-1H-pyrrol-3-yl)-5-fluorophenyl)piperazin-1-yl)phenyl)-4-fluoro-3-(trifluoromethylsulfonyl)benzenesulfonamide

: 1391107-89-3
C₅₃H₅₉ClF₄N₆O₇S₄

Guidance literature:: With N-ethyl-N,N-diisopropylamine; In N,N-dimethyl-formamide; at 20 ℃; Inert atmosphere;

Reference yield:

: 188813-02-7
3-bromo-5-fluorobenzaldehyde

: 1391107-89-3
C₅₃H₅₉ClF₄N₆O₇S₄

Guidance literature:: Multi-step reaction with 11 steps

1: piperidine; acetic acid / toluene / Reflux

2: triethylamine; 3-ethyl-5-(2-hydroxyethyl)-4-methyl-1,3-thiazolium bromide / ethanol / 70 °C

3: acetic acid / methanol / 50 °C

4: copper(l) iodide; L-proline; potassium carbonate / dimethyl sulfoxide / 120 °C

5: sodium hydroxide; water / ethanol; 1,4-dioxane / 48 h / Reflux

6: trifluoroacetic acid / dichloromethane

7: N-iodo-succinimide / N,N-dimethyl-formamide / 0 °C

8: copper(l) iodide; L-proline; sodium hydroxide / dimethyl sulfoxide / 90 °C / Inert atmosphere

9: ammonium chloride; iron / ethanol / Reflux

10: pyridine / dichloromethane / -5 °C

11: N-ethyl-N,N-diisopropylamine / N,N-dimethyl-formamide / 20 °C / Inert atmosphere

With piperidine; pyridine; N-iodo-succinimide; copper(l) iodide; water; iron; 3-ethyl-5-(2-hydroxyethyl)-4-methyl-1,3-thiazolium bromide; potassium carbonate; ammonium chloride; acetic acid; triethylamine; N-ethyl-N,N-diisopropylamine; trifluoroacetic acid; L-proline; sodium hydroxide; In 1,4-dioxane; methanol; ethanol; dichloromethane; dimethyl sulfoxide; N,N-dimethyl-formamide; toluene;

Reference yield:

: ethyl-2-(3-bromo-5-fluorobenzylidene)-3-oxobutanoate

: 1391107-89-3
C₅₃H₅₉ClF₄N₆O₇S₄

Guidance literature:: Multi-step reaction with 10 steps

1: triethylamine; 3-ethyl-5-(2-hydroxyethyl)-4-methyl-1,3-thiazolium bromide / ethanol / 70 °C

2: acetic acid / methanol / 50 °C

3: copper(l) iodide; L-proline; potassium carbonate / dimethyl sulfoxide / 120 °C

4: sodium hydroxide; water / ethanol; 1,4-dioxane / 48 h / Reflux

5: trifluoroacetic acid / dichloromethane

6: N-iodo-succinimide / N,N-dimethyl-formamide / 0 °C

7: copper(l) iodide; L-proline; sodium hydroxide / dimethyl sulfoxide / 90 °C / Inert atmosphere

8: ammonium chloride; iron / ethanol / Reflux

9: pyridine / dichloromethane / -5 °C

10: N-ethyl-N,N-diisopropylamine / N,N-dimethyl-formamide / 20 °C / Inert atmosphere

With pyridine; N-iodo-succinimide; copper(l) iodide; water; iron; 3-ethyl-5-(2-hydroxyethyl)-4-methyl-1,3-thiazolium bromide; potassium carbonate; ammonium chloride; acetic acid; triethylamine; N-ethyl-N,N-diisopropylamine; trifluoroacetic acid; L-proline; sodium hydroxide; In 1,4-dioxane; methanol; ethanol; dichloromethane; dimethyl sulfoxide; N,N-dimethyl-formamide;