benzyl N-tert-butoxycarbonyl-2-amino-5-diethoxyphosphonate-L-valeric ester

Base Information

Chemical Name:benzyl N-tert-butoxycarbonyl-2-amino-5-diethoxyphosphonate-L-valeric ester
CAS No.:125982-84-5
Molecular Formula:C₂₁H₃₄NO₇P
Molecular Weight:443.477
Hs Code.:

Synonyms:benzyl N-tert-butoxycarbonyl-2-amino-5-diethoxyphosphonate-L-valeric ester

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Chemical Property of benzyl N-tert-butoxycarbonyl-2-amino-5-diethoxyphosphonate-L-valeric ester

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Technology Process of benzyl N-tert-butoxycarbonyl-2-amino-5-diethoxyphosphonate-L-valeric ester

There total 3 articles about benzyl N-tert-butoxycarbonyl-2-amino-5-diethoxyphosphonate-L-valeric ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

: 125982-83-4,141270-57-7,141270-58-8
benzyl N-tert-butoxycarbonyl-2-amino-5-diethoxyphosphonate-5-thio-(2'-pyridyl)-L-valeric ester

: 125982-84-5
benzyl N-tert-butoxycarbonyl-2-amino-5-diethoxyphosphonate-L-valeric ester

Guidance literature:: With azobisisobutyronitrile; tri-n-butyl-tin hydride; In benzene; for 24h; Heating;
DOI:10.1016/S0040-4020(01)88721-4

Reference yield:

: 124747-27-9
2-tert-Butoxycarbonylamino-succinic acid 1-benzyl ester 4-(2-thioxo-2H-pyridin-1-yl) ester

: 125982-84-5
benzyl N-tert-butoxycarbonyl-2-amino-5-diethoxyphosphonate-L-valeric ester

Guidance literature:: Multi-step reaction with 2 steps

1: 0.712 g / tetrahydrofuran / 0.5 h / 0 °C / Irradiation

2: 88 percent / tributyltin hydride, α,α'-azoisobutyronitrile / benzene / 24 h / Heating

With azobisisobutyronitrile; tri-n-butyl-tin hydride; In tetrahydrofuran; benzene;
DOI:10.1016/S0040-4020(01)88721-4

Reference yield:

: 30925-18-9,92828-64-3,145126-18-7
2-tert-Butoxycarbonylamino-succinic acid 1-benzyl ester

: 125982-84-5
benzyl N-tert-butoxycarbonyl-2-amino-5-diethoxyphosphonate-L-valeric ester

Guidance literature:: Multi-step reaction with 3 steps

1: 1.) isobutyl chloroformate, N-methylmorpholine / 1.) 0 deg C, 15 min., THF, 2.) THF, 0 deg C, 1 h

2: 0.712 g / tetrahydrofuran / 0.5 h / 0 °C / Irradiation

3: 88 percent / tributyltin hydride, α,α'-azoisobutyronitrile / benzene / 24 h / Heating

With 4-methyl-morpholine; azobisisobutyronitrile; tri-n-butyl-tin hydride; isobutyl chloroformate; In tetrahydrofuran; benzene;
DOI:10.1016/S0040-4020(01)88721-4