((2R,3R)-3-((4-methylbenzoyl)oxy)-5-(pyren-1-yl)tetrahydrofuran-2-yl)methyl 4-methylbenzoate

Base Information

• Chemical Name: ((2R,3R)-3-((4-methylbenzoyl)oxy)-5-(pyren-1-yl)tetrahydrofuran-2-yl)methyl 4-methylbenzoate
• CAS No.: 180737-30-8
• Molecular Formula: C₃₇H₃₀O₅
• Molecular Weight: 554.642

Synonyms:((2R,3R)-3-((4-methylbenzoyl)oxy)-5-(pyren-1-yl)tetrahydrofuran-2-yl)methyl 4-methylbenzoate

Chemical Property of ((2R,3R)-3-((4-methylbenzoyl)oxy)-5-(pyren-1-yl)tetrahydrofuran-2-yl)methyl 4-methylbenzoate

Chemical Property:

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Technology Process of ((2R,3R)-3-((4-methylbenzoyl)oxy)-5-(pyren-1-yl)tetrahydrofuran-2-yl)methyl 4-methylbenzoate

There total 10 articles about ((2R,3R)-3-((4-methylbenzoyl)oxy)-5-(pyren-1-yl)tetrahydrofuran-2-yl)methyl 4-methylbenzoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 48.0%

C32H18Cd (620607-29-6) + 2-deoxy-3,5-di-O-p-toluoyl-α-D-erythro-pentofuranosyl chloride (4330-21-6) → ((2R,3R)-3-((4-methylbenzoyl)oxy)-5-(pyren-1-yl)tetrahydrofuran-2-yl)methyl 4-methylbenzoate (180737-30-8)

Guidance literature:

In tetrahydrofuran; at 20 ℃; for 4h;

Reference yield: 29.0%

((2R,3R,5R)-3-((4-methylbenzoyl)oxy)-5-(pyren-1-yl)tetrahydrofuran-2-yl)methyl 4-methylbenzoate (180854-12-0) → ((2R,3R)-3-((4-methylbenzoyl)oxy)-5-(pyren-1-yl)tetrahydrofuran-2-yl)methyl 4-methylbenzoate (180737-30-8)

Guidance literature:

With trifluoroacetic acid; In dichloromethane; at 25 ℃; for 18h; Equilibrium constant; Kinetics;

DOI:10.1016/S0040-4039(02)02481-4

Reference yield: 22.0%

pyrene (129-00-0) + 2-deoxy-3,5-di-O-p-toluoyl-α-D-erythro-pentofuranosyl chloride (4330-21-6) → (2R,3S)-2-hydroxy-5,5-dipyrenylpentyl 1,3-ditoluoate + ((2R,3R,5R)-3-((4-methylbenzoyl)oxy)-5-(pyren-1-yl)tetrahydrofuran-2-yl)methyl 4-methylbenzoate (180854-12-0) + ((2R,3R)-3-((4-methylbenzoyl)oxy)-5-(pyren-1-yl)tetrahydrofuran-2-yl)methyl 4-methylbenzoate (180737-30-8)

Guidance literature:

With silver tetrafluoroborate; In 1,2-dichloro-ethane; for 1h;

DOI:10.1039/b509846g

upstream raw materials:

1-bromopyrene

2-deoxy-3,5-di-O-p-toluoyl-α-D-erythro-pentofuranosyl chloride

((2R,3R,5R)-3-((4-methylbenzoyl)oxy)-5-(pyren-1-yl)tetrahydrofuran-2-yl)methyl 4-methylbenzoate

methyl 3,5-di-O-toluoyl-2-deoxy-D-ribofuranose

Downstream raw materials:

(2R,5R)-2-((bis(4-methoxyphenyl)(phenyl)methoxy)methyl)-5-(pyren-1-yl)tetrahydrofuran-3-ol

((2R,3R,5R)-3-((4-methylbenzoyl)oxy)-5-(pyren-1-yl)tetrahydrofuran-2-yl)methyl 4-methylbenzoate

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