(S)-(+)-N-((1E)-{1-benzyl-3-[2-(benzyloxy)ethyl]-1H-indol-2-yl}methylidene)-4-methylbenzenesulfinamide

Base Information

Chemical Name:(S)-(+)-N-((1E)-{1-benzyl-3-[2-(benzyloxy)ethyl]-1H-indol-2-yl}methylidene)-4-methylbenzenesulfinamide
CAS No.:915415-67-7
Molecular Formula:C₃₂H₃₀N₂O₂S
Molecular Weight:506.668
Hs Code.:

Synonyms:(S)-(+)-N-((1E)-{1-benzyl-3-[2-(benzyloxy)ethyl]-1H-indol-2-yl}methylidene)-4-methylbenzenesulfinamide

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Chemical Property of (S)-(+)-N-((1E)-{1-benzyl-3-[2-(benzyloxy)ethyl]-1H-indol-2-yl}methylidene)-4-methylbenzenesulfinamide

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Technology Process of (S)-(+)-N-((1E)-{1-benzyl-3-[2-(benzyloxy)ethyl]-1H-indol-2-yl}methylidene)-4-methylbenzenesulfinamide

There total 4 articles about (S)-(+)-N-((1E)-{1-benzyl-3-[2-(benzyloxy)ethyl]-1H-indol-2-yl}methylidene)-4-methylbenzenesulfinamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 76.0%

: 915415-65-5
1-benzyl-3-(2-(benzyloxy)ethyl)-1H-indole-2-carbaldehyde

: 188447-91-8
(S)-p-toluenesulfinimide

: 915415-67-7
(S)-(+)-N-((1E)-{1-benzyl-3-[2-(benzyloxy)ethyl]-1H-indol-2-yl}methylidene)-4-methylbenzenesulfinamide

Guidance literature:: With titanium(IV) tetraethanolate; In dichloromethane; for 20h; Heating;
DOI:10.1021/jo061443+

Reference yield:

: 526-55-6,930395-07-6
2-(3-indole)-ethanol

: 915415-67-7
(S)-(+)-N-((1E)-{1-benzyl-3-[2-(benzyloxy)ethyl]-1H-indol-2-yl}methylidene)-4-methylbenzenesulfinamide

Guidance literature:: Multi-step reaction with 3 steps

1: 95 percent / NaH / dimethylformamide / 0 - 20 °C

2: 95 percent / POCl₃ / 12 h / 60 °C

3: 76 percent / Ti(OEt)4 / CH₂Cl₂ / 20 h / Heating

With titanium(IV) tetraethanolate; sodium hydride; trichlorophosphate; In dichloromethane; N,N-dimethyl-formamide; 2: Vilsmeier formylation reaction;
DOI:10.1021/jo061443+

Reference yield:

: 100-39-0
benzyl bromide

: 915415-67-7
(S)-(+)-N-((1E)-{1-benzyl-3-[2-(benzyloxy)ethyl]-1H-indol-2-yl}methylidene)-4-methylbenzenesulfinamide

Guidance literature:: Multi-step reaction with 3 steps

1: 95 percent / NaH / dimethylformamide / 0 - 20 °C

2: 95 percent / POCl₃ / 12 h / 60 °C

3: 76 percent / Ti(OEt)4 / CH₂Cl₂ / 20 h / Heating

With titanium(IV) tetraethanolate; sodium hydride; trichlorophosphate; In dichloromethane; N,N-dimethyl-formamide; 2: Vilsmeier formylation reaction;
DOI:10.1021/jo061443+