N₂,N₂-Dibenzyl-N₄-(6-methyl-pyridin-3-ylmethyl)-3-nitro-6-oxazol-2-yl-pyridine-2,4-diamine

Base Information

• Chemical Name: N₂,N₂-Dibenzyl-N₄-(6-methyl-pyridin-3-ylmethyl)-3-nitro-6-oxazol-2-yl-pyridine-2,4-diamine
• CAS No.: 947146-15-8
• Molecular Formula: C₂₉H₂₆N₆O₃
• Molecular Weight: 506.564

Synonyms:N₂,N₂-Dibenzyl-N₄-(6-methyl-pyridin-3-ylmethyl)-3-nitro-6-oxazol-2-yl-pyridine-2,4-diamine

Chemical Property of N₂,N₂-Dibenzyl-N₄-(6-methyl-pyridin-3-ylmethyl)-3-nitro-6-oxazol-2-yl-pyridine-2,4-diamine

Chemical Property:

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Technology Process of N₂,N₂-Dibenzyl-N₄-(6-methyl-pyridin-3-ylmethyl)-3-nitro-6-oxazol-2-yl-pyridine-2,4-diamine

There total 1 articles about N₂,N₂-Dibenzyl-N₄-(6-methyl-pyridin-3-ylmethyl)-3-nitro-6-oxazol-2-yl-pyridine-2,4-diamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

oxazol (288-42-6) + N2,N2-dibenzyl-6-bromo-N4-(6-methyl-pyridin-3-ylmethyl)-3-nitropyridine-2,4-diamine (947146-11-4) → N2,N2-Dibenzyl-N4-(6-methyl-pyridin-3-ylmethyl)-3-nitro-6-oxazol-2-yl-pyridine-2,4-diamine (947146-15-8)

Guidance literature:

oxazol; With n-butyllithium; In tetrahydrofuran; at -78 - -60 ℃; for 0.166667h; Cooling with acetone-dry ice;

With zinc(II) chloride; In tetrahydrofuran; at -78 - 20 ℃;

N₂,N₂-dibenzyl-6-bromo-N₄-(6-methyl-pyridin-3-ylmethyl)-3-nitropyridine-2,4-diamine; bis-triphenylphosphine-palladium(II) chloride; In tetrahydrofuran; at 130 ℃; for 0.25h; Microwave irradiation;

Reference yield:

N2,N2-Dibenzyl-N4-(6-methyl-pyridin-3-ylmethyl)-3-nitro-6-oxazol-2-yl-pyridine-2,4-diamine (947146-15-8) → N2,N2-dibenzyl-N4-(6-methyl-pyridin-3-ylmethyl)-6-oxazol-2-yl-pyridine-2,3,4-triamine (947143-88-6)

Guidance literature:

With hydrogen; Raney Nickel; In tetrahydrofuran; methanol; at 20 ℃; for 1h; under 4137.29 Torr;

upstream raw materials:

oxazol

N₂,N₂-dibenzyl-6-bromo-N₄-(6-methyl-pyridin-3-ylmethyl)-3-nitropyridine-2,4-diamine

Downstream raw materials:

N₂,N₂-dibenzyl-N₄-(6-methyl-pyridin-3-ylmethyl)-6-oxazol-2-yl-pyridine-2,3,4-triamine

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