1-(3-bromobenzyl)-5-(1-hydroxy-3-(((4-methoxybenzyl)oxy)imino)-3-(4-(trifluoromethoxy)phenyl)propyl)pyridin-2(1H)-one

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Chemical Name:1-(3-bromobenzyl)-5-(1-hydroxy-3-(((4-methoxybenzyl)oxy)imino)-3-(4-(trifluoromethoxy)phenyl)propyl)pyridin-2(1H)-one
CAS No.:1571034-47-3
Molecular Formula:C₃₀H₂₆BrF₃N₂O₅
Molecular Weight:631.446
Hs Code.:

Synonyms:1-(3-bromobenzyl)-5-(1-hydroxy-3-(((4-methoxybenzyl)oxy)imino)-3-(4-(trifluoromethoxy)phenyl)propyl)pyridin-2(1H)-one

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Chemical Property of 1-(3-bromobenzyl)-5-(1-hydroxy-3-(((4-methoxybenzyl)oxy)imino)-3-(4-(trifluoromethoxy)phenyl)propyl)pyridin-2(1H)-one

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Technology Process of 1-(3-bromobenzyl)-5-(1-hydroxy-3-(((4-methoxybenzyl)oxy)imino)-3-(4-(trifluoromethoxy)phenyl)propyl)pyridin-2(1H)-one

There total 5 articles about 1-(3-bromobenzyl)-5-(1-hydroxy-3-(((4-methoxybenzyl)oxy)imino)-3-(4-(trifluoromethoxy)phenyl)propyl)pyridin-2(1H)-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 60.0%

: 1571034-51-9
C₁₇H₁₆F₃NO₃

: 1571034-45-1
1-(3-bromobenzyl)-6-oxo-1,6-dihydropyridine-3-carbaldehyde

: 1571034-47-3
1-(3-bromobenzyl)-5-(1-hydroxy-3-(((4-methoxybenzyl)oxy)imino)-3-(4-(trifluoromethoxy)phenyl)propyl)pyridin-2(1H)-one

Guidance literature:: C₁₇H₁₆F₃NO₃; With n-butyllithium; In tetrahydrofuran; hexane; at -78 ℃; for 1h;

1-(3-bromobenzyl)-6-oxo-1,6-dihydropyridine-3-carbaldehyde; In tetrahydrofuran; hexane; at -78 ℃; for 6h;

Reference yield:

: 823-78-9
meta-bromobenzyl bromide

: 1571034-47-3
1-(3-bromobenzyl)-5-(1-hydroxy-3-(((4-methoxybenzyl)oxy)imino)-3-(4-(trifluoromethoxy)phenyl)propyl)pyridin-2(1H)-one

Guidance literature:: Multi-step reaction with 2 steps

1.1: caesium carbonate; lithium chloride / N,N-dimethyl-formamide / 18 h / 65 °C

2.1: n-butyllithium / tetrahydrofuran; hexane / 1 h / -78 °C

2.2: 6 h / -78 °C

With n-butyllithium; caesium carbonate; lithium chloride; In tetrahydrofuran; hexane; N,N-dimethyl-formamide;

Reference yield:

: 85013-98-5
1-[4-(trifluoromethoxy)phenyl]ethan-1-one

: 1571034-47-3
1-(3-bromobenzyl)-5-(1-hydroxy-3-(((4-methoxybenzyl)oxy)imino)-3-(4-(trifluoromethoxy)phenyl)propyl)pyridin-2(1H)-one

Guidance literature:: Multi-step reaction with 2 steps

1.1: pyridine / 18 h / 20 °C

2.1: n-butyllithium / tetrahydrofuran; hexane / 1 h / -78 °C

2.2: 6 h / -78 °C

With n-butyllithium; In tetrahydrofuran; pyridine; hexane;