p-trifluoroacetamidophenyl 2-acetamido-2-deoxy-6-O-α-D-glucopyranosyl-β-D-glucopyranoside

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Chemical Name:p-trifluoroacetamidophenyl 2-acetamido-2-deoxy-6-O-α-D-glucopyranosyl-β-D-glucopyranoside
CAS No.:86204-00-4
Molecular Formula:C₂₂H₂₉F₃N₂O₁₂
Molecular Weight:570.474
Hs Code.:

Synonyms:p-trifluoroacetamidophenyl 2-acetamido-2-deoxy-6-O-α-D-glucopyranosyl-β-D-glucopyranoside

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Chemical Property of p-trifluoroacetamidophenyl 2-acetamido-2-deoxy-6-O-α-D-glucopyranosyl-β-D-glucopyranoside

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Technology Process of p-trifluoroacetamidophenyl 2-acetamido-2-deoxy-6-O-α-D-glucopyranosyl-β-D-glucopyranoside

There total 5 articles about p-trifluoroacetamidophenyl 2-acetamido-2-deoxy-6-O-α-D-glucopyranosyl-β-D-glucopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

: 86203-99-8
p-trifluoroacetamidophenyl 2-acetamido-3,4-di-O-benzoyl-2-deoxy-6-O-(2,3,4,6-tetra-O-benzyl-α-D-glucopyranosyl)-β-D-glucopyranoside

: 86204-00-4
p-trifluoroacetamidophenyl 2-acetamido-2-deoxy-6-O-α-D-glucopyranosyl-β-D-glucopyranoside

Guidance literature:: With hydrogen; palladium on activated charcoal; In ethanol; for 16h; under 3000.2 Torr;
DOI:10.1016/S0008-6215(00)90951-0

Reference yield:

: 4196-35-4
2,3,4,6-tetra-O-benzyl-α-D-glucopyranosyl bromide

: 86204-00-4
p-trifluoroacetamidophenyl 2-acetamido-2-deoxy-6-O-α-D-glucopyranosyl-β-D-glucopyranoside

Guidance literature:: Multi-step reaction with 2 steps

1: 81 percent / tetraethylammonium bromide, molecular sieves / dimethylformamide; CH₂Cl₂ / 24 h / Ambient temperature

2: 88 percent / hydrogen / 10 percent Pd/C / ethanol / 16 h / 3000.2 Torr

With molecular sieve; tetraethylammonium bromide; hydrogen; palladium on activated charcoal; In ethanol; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1016/S0008-6215(00)90951-0

Reference yield:

: 84564-19-2
p-nitrophenyl 2-acetamido-3,4-di-O-benzoyl-2-deoxy-6-O-trityl-β-D-glucopyranoside

: 86204-00-4
p-trifluoroacetamidophenyl 2-acetamido-2-deoxy-6-O-α-D-glucopyranosyl-β-D-glucopyranoside

Guidance literature:: Multi-step reaction with 4 steps

1: 1.) hydrogen / 1.) Adams' catalyst / 1.) ethyl acetate; 2.) pyridine, -10 deg C, 60 min

2: 65 percent / 80 percent acetic acid / H₂O / 0.5 h / 80 °C

3: 81 percent / tetraethylammonium bromide, molecular sieves / dimethylformamide; CH₂Cl₂ / 24 h / Ambient temperature

4: 88 percent / hydrogen / 10 percent Pd/C / ethanol / 16 h / 3000.2 Torr

With molecular sieve; tetraethylammonium bromide; hydrogen; acetic acid; platinum(IV) oxide; palladium on activated charcoal; In ethanol; dichloromethane; water; N,N-dimethyl-formamide;
DOI:10.1016/S0008-6215(00)90951-0