(S)-2-[(S)-2-Amino-3-(4-benzyloxy-phenyl)-propionylamino]-3-(4-hydroxy-3,5-diiodo-phenyl)-propionic acid methyl ester; hydrochloride

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Chemical Name:(S)-2-[(S)-2-Amino-3-(4-benzyloxy-phenyl)-propionylamino]-3-(4-hydroxy-3,5-diiodo-phenyl)-propionic acid methyl ester; hydrochloride
CAS No.:123418-37-1
Molecular Formula:C₂₆H₂₆I₂N₂O₅*ClH
Molecular Weight:736.773
Hs Code.:

Synonyms:(S)-2-[(S)-2-Amino-3-(4-benzyloxy-phenyl)-propionylamino]-3-(4-hydroxy-3,5-diiodo-phenyl)-propionic acid methyl ester; hydrochloride

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Chemical Property of (S)-2-[(S)-2-Amino-3-(4-benzyloxy-phenyl)-propionylamino]-3-(4-hydroxy-3,5-diiodo-phenyl)-propionic acid methyl ester; hydrochloride

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Technology Process of (S)-2-[(S)-2-Amino-3-(4-benzyloxy-phenyl)-propionylamino]-3-(4-hydroxy-3,5-diiodo-phenyl)-propionic acid methyl ester; hydrochloride

There total 3 articles about (S)-2-[(S)-2-Amino-3-(4-benzyloxy-phenyl)-propionylamino]-3-(4-hydroxy-3,5-diiodo-phenyl)-propionic acid methyl ester; hydrochloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: (S)-2-[(S)-3-(4-Benzyloxy-phenyl)-2-tert-butoxycarbonylamino-propionylamino]-3-(4-hydroxy-3,5-diiodo-phenyl)-propionic acid methyl ester

: 123418-37-1
(S)-2-[(S)-2-Amino-3-(4-benzyloxy-phenyl)-propionylamino]-3-(4-hydroxy-3,5-diiodo-phenyl)-propionic acid methyl ester; hydrochloride

Guidance literature:: With hydrogenchloride; In 1,4-dioxane; Yield given; Ambient temperature; overnight;
DOI:10.1016/S0040-4039(00)95207-9

Reference yield:

: 2130-96-3,54784-43-9
O-benzyl-N-tert-butoxycarbonyl-L-tyrosine

: 123418-37-1
(S)-2-[(S)-2-Amino-3-(4-benzyloxy-phenyl)-propionylamino]-3-(4-hydroxy-3,5-diiodo-phenyl)-propionic acid methyl ester; hydrochloride

Guidance literature:: Multi-step reaction with 2 steps

1: DCC, 1-hydroxybenztriazole, N-methylmorpholine / dimethylformamide / 0 deg C to room temp., overnight

2: HCl / dioxane / Ambient temperature; overnight

With 4-methyl-morpholine; hydrogenchloride; benzotriazol-1-ol; dicyclohexyl-carbodiimide; In 1,4-dioxane; N,N-dimethyl-formamide;
DOI:10.1016/S0040-4039(00)95207-9

Reference yield:

: 76318-50-8
3,5-diiodo-L-thyrosine methyl ester

: 123418-37-1
(S)-2-[(S)-2-Amino-3-(4-benzyloxy-phenyl)-propionylamino]-3-(4-hydroxy-3,5-diiodo-phenyl)-propionic acid methyl ester; hydrochloride

Guidance literature:: Multi-step reaction with 2 steps

1: DCC, 1-hydroxybenztriazole, N-methylmorpholine / dimethylformamide / 0 deg C to room temp., overnight

2: HCl / dioxane / Ambient temperature; overnight

With 4-methyl-morpholine; hydrogenchloride; benzotriazol-1-ol; dicyclohexyl-carbodiimide; In 1,4-dioxane; N,N-dimethyl-formamide;
DOI:10.1016/S0040-4039(00)95207-9