cyclohexyl phenyl silane diol

Base Information

Chemical Name:cyclohexyl phenyl silane diol
CAS No.:18053-86-6
Molecular Formula:C₁₂H₁₈O₂Si
Molecular Weight:222.359
Hs Code.:

Synonyms:cyclohexyl phenyl silane diol

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Chemical Property of cyclohexyl phenyl silane diol

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Technology Process of cyclohexyl phenyl silane diol

There total 4 articles about cyclohexyl phenyl silane diol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 931-50-0
cyclohexylmagnesium bromide

: 18053-86-6
cyclohexyl phenyl silane diol

Guidance literature:: Multi-step reaction with 2 steps

1: diethyl ether; benzene / Erhitzen des von den Loesungsmitteln befreiten Reaktionsgemisches auf 100grad

2: aqueous KOH-solution

With potassium hydroxide; diethyl ether; benzene;
DOI:10.1039/jr9320002205

Reference yield:

: 18042-67-6
(dichloro)(cyclohexyl)(phenyl)silane

: 18053-86-6
cyclohexyl phenyl silane diol

Guidance literature:: With potassium hydroxide;
DOI:10.1039/jr9320002205

Reference yield:

: 108-85-0
1-bromocyclohexane

: 98-13-5
Phenyltrichlorosilane

: 18053-86-6
cyclohexyl phenyl silane diol

Guidance literature:: Multi-step reaction with 2 steps

1.1: magnesium; iodine / tetrahydrofuran / 0.5 h / Inert atmosphere; Reflux

1.2: 13 h / -78 - 20 °C / Inert atmosphere

1.3: 3 h / 20 °C / Inert atmosphere

2.1: C₂₀H₂₄MnN₈O₂⁽²⁺⁾*2ClO₄^(1-)*2H₂O; dihydrogen peroxide / acetone / 2 h / 20 °C / Green chemistry

With C₂₀H₂₄MnN₈O₂⁽²⁺⁾*2ClO₄^(1-)*2H₂O; dihydrogen peroxide; iodine; magnesium; In tetrahydrofuran; acetone;
DOI:10.1002/anie.201900342