N,N′-bis(2,4-dibutoxybenzyl)-1,7-dibromo-3,4:9,10-perylenetetracarboxylic diimide

Base Information

Chemical Name:N,N′-bis(2,4-dibutoxybenzyl)-1,7-dibromo-3,4:9,10-perylenetetracarboxylic diimide
CAS No.:1224931-22-9
Molecular Formula:C₅₄H₅₂Br₂N₂O₈
Molecular Weight:1016.82
Hs Code.:

Synonyms:N,N′-bis(2,4-dibutoxybenzyl)-1,7-dibromo-3,4:9,10-perylenetetracarboxylic diimide

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Chemical Property of N,N′-bis(2,4-dibutoxybenzyl)-1,7-dibromo-3,4:9,10-perylenetetracarboxylic diimide

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Technology Process of N,N′-bis(2,4-dibutoxybenzyl)-1,7-dibromo-3,4:9,10-perylenetetracarboxylic diimide

There total 1 articles about N,N′-bis(2,4-dibutoxybenzyl)-1,7-dibromo-3,4:9,10-perylenetetracarboxylic diimide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1225456-18-7
2,4-di-n-butoxybenzylamine

: 128-69-8
perylene-3,4,9,10-tetracarboxylic acid 3,4:9,10-dianhydride

: 1224931-22-9
N,N′-bis(2,4-dibutoxybenzyl)-1,7-dibromo-3,4:9,10-perylenetetracarboxylic diimide

: 1426664-29-0
N,N′-bis(2,4-dibutoxybenzyl)-1,6-dibromo-3,4:9,10-perylenetetracarboxylic diimide

Guidance literature:: perylene-3,4,9,10-tetracarboxylic acid 3,4:9,10-dianhydride; Inert atmosphere;

2,4-di-n-butoxybenzylamine; Inert atmosphere;
DOI:10.1002/anie.200905503

Reference yield: 69.0%

: 1224931-22-9
N,N′-bis(2,4-dibutoxybenzyl)-1,7-dibromo-3,4:9,10-perylenetetracarboxylic diimide

: 4334-88-7
p-ethoxycarbonylphenylboronic acid

: 1224931-21-8
N,N'-di(2,4-dibutoxybenzyl)-1,7-di(4-(ethoxycarbonyl)phenyl)perylene-3,4:9,10-tetracarboxylic diimide

Guidance literature:: With tetrakis(triphenylphosphine) palladium⁽⁰⁾; cesium fluoride; silver(l) oxide; In toluene; at 70 - 80 ℃; Inert atmosphere;
DOI:10.1039/b926824c