ethyl 2,2,2-trichloro-1-[2-(2,3-dibromopropoxy)phenyl]ethyl carbonate

Base Information

Chemical Name:ethyl 2,2,2-trichloro-1-[2-(2,3-dibromopropoxy)phenyl]ethyl carbonate
CAS No.:1620143-60-3
Molecular Formula:C₁₄H₁₅Br₂Cl₃O₄
Molecular Weight:513.438
Hs Code.:

Synonyms:ethyl 2,2,2-trichloro-1-[2-(2,3-dibromopropoxy)phenyl]ethyl carbonate

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Chemical Property of ethyl 2,2,2-trichloro-1-[2-(2,3-dibromopropoxy)phenyl]ethyl carbonate

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Technology Process of ethyl 2,2,2-trichloro-1-[2-(2,3-dibromopropoxy)phenyl]ethyl carbonate

There total 3 articles about ethyl 2,2,2-trichloro-1-[2-(2,3-dibromopropoxy)phenyl]ethyl carbonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

: 56-23-5
tetrachloromethane

: 1620143-59-0
ethyl 2,2,2-trichloro-1-(2-allyloxyphenyl)ethyl carbonate

: 1620143-60-3
ethyl 2,2,2-trichloro-1-[2-(2,3-dibromopropoxy)phenyl]ethyl carbonate

Guidance literature:: With bromine; at -5 - 0 ℃; for 2h;
DOI:10.1016/j.tetlet.2014.05.097

Reference yield:

: 28752-82-1
2-(allyloxy)benzaldehyde

: 1620143-60-3
ethyl 2,2,2-trichloro-1-[2-(2,3-dibromopropoxy)phenyl]ethyl carbonate

Guidance literature:: Multi-step reaction with 2 steps

1: 1,8-diazabicyclo[5.4.0]undec-7-ene; triethylamine / chloroform / 4 h / 0 - 30 °C

2: bromine / 2 h / -5 - 0 °C

With bromine; 1,8-diazabicyclo[5.4.0]undec-7-ene; triethylamine; In chloroform;
DOI:10.1016/j.tetlet.2014.05.097

Reference yield:

: 90-02-8
salicylaldehyde

: 1620143-60-3
ethyl 2,2,2-trichloro-1-[2-(2,3-dibromopropoxy)phenyl]ethyl carbonate

Guidance literature:: Multi-step reaction with 3 steps

1: sodium hydride / N,N-dimethyl-formamide; tetrahydrofuran / 4 h / 25 °C

2: 1,8-diazabicyclo[5.4.0]undec-7-ene; triethylamine / chloroform / 4 h / 0 - 30 °C

3: bromine / 2 h / -5 - 0 °C

With bromine; sodium hydride; 1,8-diazabicyclo[5.4.0]undec-7-ene; triethylamine; In tetrahydrofuran; chloroform; N,N-dimethyl-formamide;
DOI:10.1016/j.tetlet.2014.05.097