C₃₁H₄₁NO₃Si

Base Information

Chemical Name:C₃₁H₄₁NO₃Si
CAS No.:1312542-28-1
Molecular Formula:C₃₁H₄₁NO₃Si
Molecular Weight:503.757
Hs Code.:

C<sub>31</sub>H<sub>41</sub>NO<sub>3</sub>Si

Synonyms:C₃₁H₄₁NO₃Si

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Chemical Property of C₃₁H₄₁NO₃Si

Chemical Property:

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Technology Process of C₃₁H₄₁NO₃Si

There total 12 articles about C₃₁H₄₁NO₃Si which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

: 1312542-27-0
C₃₀H₃₉NO₃Si

: 74-88-4
methyl iodide

: 1312542-28-1
C₃₁H₄₁NO₃Si

Guidance literature:: C₃₀H₃₉NO₃Si; With potassium hydride; In tetrahydrofuran; mineral oil; at 0 - 25 ℃; for 0.5h;

methyl iodide; In tetrahydrofuran; mineral oil; at 25 ℃; for 1.5h;
DOI:10.1021/ol201095b

Reference yield:

: 1199940-92-5
C₁₄H₂₄O₃Si

: 1312542-28-1
C₃₁H₄₁NO₃Si

Guidance literature:: Multi-step reaction with 11 steps

1.1: dichloromethane / 24 h / 25 °C / Inert atmosphere

2.1: diisobutylaluminium hydride / dichloromethane / 0.5 h / -30 °C / Inrtert atmosphere

3.1: 2,6-dimethylpyridine / dichloromethane / 2 h / 0 - 25 °C

4.1: N,N,N,N,N,N-hexamethylphosphoric triamide; samarium diiodide / tetrahydrofuran / 0.33 h / -20 °C

4.2: 0.5 h / -20 - 25 °C

5.1: hydrogenchloride / 72 h / 120 °C / Inert atmosphere; Molecular sieve

6.1: pyridine / 6 h / 25 °C

7.1: 2 h / 180 °C / vacuum

8.1: tetrahydrofuran / 0.5 h / -30 °C

9.1: potassium hexamethylsilazane / diethylene glycol dimethyl ether; toluene / 1 h / 95 °C / Inert atmosphere

10.1: tetramethylammonium borohydride / tetrahydrofuran; water / 0.5 h / 0 °C

11.1: potassium hydride / tetrahydrofuran; mineral oil / 0.5 h / 0 - 25 °C

11.2: 1.5 h / 25 °C

With pyridine; 2,6-dimethylpyridine; hydrogenchloride; N,N,N,N,N,N-hexamethylphosphoric triamide; samarium diiodide; tetramethylammonium borohydride; potassium hydride; potassium hexamethylsilazane; diisobutylaluminium hydride; In tetrahydrofuran; dichloromethane; diethylene glycol dimethyl ether; water; toluene; mineral oil;
DOI:10.1021/ol201095b

Reference yield:

: 1312542-05-4
C₃₀H₃₅NO₇SSi

: 1312542-28-1
C₃₁H₄₁NO₃Si

Guidance literature:: Multi-step reaction with 10 steps

1.1: diisobutylaluminium hydride / dichloromethane / 0.5 h / -30 °C / Inrtert atmosphere

2.1: 2,6-dimethylpyridine / dichloromethane / 2 h / 0 - 25 °C

3.1: N,N,N,N,N,N-hexamethylphosphoric triamide; samarium diiodide / tetrahydrofuran / 0.33 h / -20 °C

3.2: 0.5 h / -20 - 25 °C

4.1: hydrogenchloride / 72 h / 120 °C / Inert atmosphere; Molecular sieve

5.1: pyridine / 6 h / 25 °C

6.1: 2 h / 180 °C / vacuum

7.1: tetrahydrofuran / 0.5 h / -30 °C

8.1: potassium hexamethylsilazane / diethylene glycol dimethyl ether; toluene / 1 h / 95 °C / Inert atmosphere

9.1: tetramethylammonium borohydride / tetrahydrofuran; water / 0.5 h / 0 °C

10.1: potassium hydride / tetrahydrofuran; mineral oil / 0.5 h / 0 - 25 °C

10.2: 1.5 h / 25 °C

With pyridine; 2,6-dimethylpyridine; hydrogenchloride; N,N,N,N,N,N-hexamethylphosphoric triamide; samarium diiodide; tetramethylammonium borohydride; potassium hydride; potassium hexamethylsilazane; diisobutylaluminium hydride; In tetrahydrofuran; dichloromethane; diethylene glycol dimethyl ether; water; toluene; mineral oil;
DOI:10.1021/ol201095b