C₁₆H₁₁BrO₂

Base Information

Chemical Name:C₁₆H₁₁BrO₂
CAS No.:1349177-77-0
Molecular Formula:C₁₆H₁₁BrO₂
Molecular Weight:315.166
Hs Code.:

C<sub>16</sub>H<sub>11</sub>BrO<sub>2</sub>

Synonyms:C₁₆H₁₁BrO₂

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Chemical Property of C₁₆H₁₁BrO₂

Chemical Property:

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Technology Process of C₁₆H₁₁BrO₂

There total 5 articles about C₁₆H₁₁BrO₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 64.0%

: C₁₀H₄BrF₃O₅S

: 5142-75-6
tri(p-tolyl)bismuth

: 1349177-77-0
C₁₆H₁₁BrO₂

Guidance literature:: With potassium phosphate; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In N,N-dimethyl-formamide; at 90 ℃; for 4h; Schlenk technique; Inert atmosphere;
DOI:10.1007/s12039-018-1565-6

Reference yield:

: 1450-75-5
5-Bromo-2-hydroxyacetophenone

: 1349177-77-0
C₁₆H₁₁BrO₂

Guidance literature:: Multi-step reaction with 5 steps

1.1: 1 h / Reflux

2.1: hydrogenchloride / dichloromethane; water / 1 h / Reflux

3.1: sodium hydroxide; dihydrogen peroxide / dichloromethane / 0 - 15 °C

3.2: 1 h / 70 °C

4.1: triethylamine / dichloromethane / 0.17 h / 0 °C

4.2: 10 h / 20 °C

5.1: tetrakis(triphenylphosphine) palladium⁽⁰⁾; potassium phosphate / N,N-dimethyl-formamide / 4 h / 90 °C / Schlenk technique; Inert atmosphere

With hydrogenchloride; potassium phosphate; tetrakis(triphenylphosphine) palladium⁽⁰⁾; dihydrogen peroxide; triethylamine; sodium hydroxide; In dichloromethane; water; N,N-dimethyl-formamide;
DOI:10.1007/s12039-018-1565-6

Reference yield:

: 6-bromo-3-hydroxy-4H-chromen-4-one

: 1349177-77-0
C₁₆H₁₁BrO₂

Guidance literature:: Multi-step reaction with 2 steps

1.1: triethylamine / dichloromethane / 0.17 h / 0 °C

1.2: 10 h / 20 °C

2.1: tetrakis(triphenylphosphine) palladium⁽⁰⁾; potassium phosphate / N,N-dimethyl-formamide / 4 h / 90 °C / Schlenk technique; Inert atmosphere

With potassium phosphate; tetrakis(triphenylphosphine) palladium⁽⁰⁾; triethylamine; In dichloromethane; N,N-dimethyl-formamide;
DOI:10.1007/s12039-018-1565-6