N¹-(1,3-dimethylimidazolidin-2-ylidene)-N²,N²-diethylbenzene-1,2-diamine

Base Information

Chemical Name:N¹-(1,3-dimethylimidazolidin-2-ylidene)-N²,N²-diethylbenzene-1,2-diamine
CAS No.:131677-20-8
Molecular Formula:C₁₅H₂₄N₄
Molecular Weight:260.382
Hs Code.:

N<SUP>1</SUP>-(1,3-dimethylimidazolidin-2-ylidene)-N<SUP>2</SUP>,N<SUP>2</SUP>-diethylbenzene-1,2-diamine

Synonyms:N¹-(1,3-dimethylimidazolidin-2-ylidene)-N²,N²-diethylbenzene-1,2-diamine

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N¹-(1,3-dimethylimidazolidin-2-ylidene)-N²,N²-diethylbenzene-1,2-diamine

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Technology Process of N¹-(1,3-dimethylimidazolidin-2-ylidene)-N²,N²-diethylbenzene-1,2-diamine

There total 3 articles about N¹-(1,3-dimethylimidazolidin-2-ylidene)-N²,N²-diethylbenzene-1,2-diamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.0%

: 19056-34-9
N¹,N¹-diethylbenzene-1,2-diamine

: 37091-73-9
2-chloro-1,3-dimethylimidazolinium chloride

: 131677-20-8
N¹-(1,3-dimethylimidazolidin-2-ylidene)-N²,N²-diethylbenzene-1,2-diamine

Guidance literature:: With triethylamine; In acetonitrile; at 0 - 80 ℃; for 5h; Inert atmosphere; Schlenk technique;
DOI:10.1002/ejic.201600870

Reference yield:

: 1493-27-2,127723-77-7
ortho-nitrofluorobenzene

: 131677-20-8
N¹-(1,3-dimethylimidazolidin-2-ylidene)-N²,N²-diethylbenzene-1,2-diamine

Guidance literature:: Multi-step reaction with 3 steps

1: potassium carbonate / dimethyl sulfoxide / 12 h / 50 °C / Inert atmosphere; Schlenk technique

2: palladium 10% on activated carbon; hydrogen / methanol / 5 h / 20 °C / Inert atmosphere; Schlenk technique

3: triethylamine / acetonitrile / 5 h / 0 - 80 °C / Inert atmosphere; Schlenk technique

With palladium 10% on activated carbon; hydrogen; potassium carbonate; triethylamine; In methanol; dimethyl sulfoxide; acetonitrile;
DOI:10.1002/ejic.201600870