tert-butyl 2-diazo-3-hydroxy-3-(2-iodo-3-methylphenyl)propionate

Base Information Edit

Chemical Name:tert-butyl 2-diazo-3-hydroxy-3-(2-iodo-3-methylphenyl)propionate
CAS No.:1044741-30-1
Molecular Formula:C₁₄H₁₇IN₂O₃
Molecular Weight:388.205
Hs Code.:
Mol file:1044741-30-1.mol

Synonyms:tert-butyl 2-diazo-3-hydroxy-3-(2-iodo-3-methylphenyl)propionate

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Chemical Property of tert-butyl 2-diazo-3-hydroxy-3-(2-iodo-3-methylphenyl)propionate Edit

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Technology Process of tert-butyl 2-diazo-3-hydroxy-3-(2-iodo-3-methylphenyl)propionate

There total 1 articles about tert-butyl 2-diazo-3-hydroxy-3-(2-iodo-3-methylphenyl)propionate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 68.0%

: 1694-31-1
tert-butyl acetoacetate

: 100130-55-0
2-iodo-3-methylbenzaldehyde

: 1044741-30-1
tert-butyl 2-diazo-3-hydroxy-3-(2-iodo-3-methylphenyl)propionate

Guidance literature:: tert-butyl acetoacetate; With sodium hydroxide; sodium azide; p-toluenesulfonyl chloride; tetrabutylammomium bromide; In diethyl ether; at 20 ℃; for 12h;

3-methyl-2-iodobenzaldehyde; In diethyl ether; water; at 0 ℃; for 1.5h; Further stages.;
DOI:10.1021/jo8010864