1-(4-methoxyphenyl)-4,4-dimethyl-1-penten-3-one oxime O-pentafluorobenzoate

Base Information

Chemical Name:1-(4-methoxyphenyl)-4,4-dimethyl-1-penten-3-one oxime O-pentafluorobenzoate
CAS No.:1028801-60-6
Molecular Formula:C₂₁H₁₈F₅NO₃
Molecular Weight:427.371
Hs Code.:

Synonyms:1-(4-methoxyphenyl)-4,4-dimethyl-1-penten-3-one oxime O-pentafluorobenzoate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1-(4-methoxyphenyl)-4,4-dimethyl-1-penten-3-one oxime O-pentafluorobenzoate

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Technology Process of 1-(4-methoxyphenyl)-4,4-dimethyl-1-penten-3-one oxime O-pentafluorobenzoate

There total 1 articles about 1-(4-methoxyphenyl)-4,4-dimethyl-1-penten-3-one oxime O-pentafluorobenzoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

: 1028801-22-0
1-(4-methoxyphenyl)-4,4-dimethyl-1-penten-3-one oxime

pentafluorobenzoylchloride: 2251-50-5
pentafluorobenzoylchloride

: 1028801-60-6
1-(4-methoxyphenyl)-4,4-dimethyl-1-penten-3-one oxime O-pentafluorobenzoate

Guidance literature:: With triethylamine; In dichloromethane; at 0 ℃; for 0.5h;
DOI:10.1021/ja8013743

Reference yield: 86.0%

: 1028801-60-6
1-(4-methoxyphenyl)-4,4-dimethyl-1-penten-3-one oxime O-pentafluorobenzoate

: 42599-18-8
(E)-1-hexenyldihydroxyborane

: 1028801-83-3
5-butyl-2-(tert-butyl)-4-(4-methoxyphenyl)-pyridine

Guidance literature:: 1-(4-methoxyphenyl)-4,4-dimethyl-1-penten-3-one oxime O-pentafluorobenzoate; (E)-1-hexenyldihydroxyborane; With copper diacetate; 4 A molecular sieve; In N,N-dimethyl-formamide; at 50 ℃; for 2h;

With air; In N,N-dimethyl-formamide; at 90 ℃; for 3h; Further stages.;
DOI:10.1021/ja8013743