Technology Process of C20H15BrN4O
There total 8 articles about C20H15BrN4O which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
potassium carbonate;
In
N,N-dimethyl acetamide;
at 80 ℃;
for 9.5h;
- Guidance literature:
-
Multi-step reaction with 6 steps
1: acetic acid / water / 4 h / 35 °C
2: trichlorophosphate; N,N-dimethyl-aniline / 2 h / 120 °C
3: sodium hydroxide / water; tetrahydrofuran / 2 h / 40 °C
4: potassium carbonate; bis-triphenylphosphine-palladium(II) chloride / water; 1,4-dioxane / 105 °C / Inert atmosphere
5: trichlorophosphate; N,N-dimethyl-aniline / 0.5 h / 120 °C
6: potassium carbonate / N,N-dimethyl acetamide / 9.5 h / 80 °C
With
bis-triphenylphosphine-palladium(II) chloride; potassium carbonate; acetic acid; N,N-dimethyl-aniline; sodium hydroxide; trichlorophosphate;
In
tetrahydrofuran; 1,4-dioxane; N,N-dimethyl acetamide; water;
- Guidance literature:
-
Multi-step reaction with 5 steps
1: trichlorophosphate; N,N-dimethyl-aniline / 2 h / 120 °C
2: sodium hydroxide / water; tetrahydrofuran / 2 h / 40 °C
3: potassium carbonate; bis-triphenylphosphine-palladium(II) chloride / water; 1,4-dioxane / 105 °C / Inert atmosphere
4: trichlorophosphate; N,N-dimethyl-aniline / 0.5 h / 120 °C
5: potassium carbonate / N,N-dimethyl acetamide / 9.5 h / 80 °C
With
bis-triphenylphosphine-palladium(II) chloride; potassium carbonate; N,N-dimethyl-aniline; sodium hydroxide; trichlorophosphate;
In
tetrahydrofuran; 1,4-dioxane; N,N-dimethyl acetamide; water;