Hydroxyamino-phenyl-acetic acid ethyl ester; hydrochloride

Base Information

Chemical Name:Hydroxyamino-phenyl-acetic acid ethyl ester; hydrochloride
CAS No.:78437-28-2
Molecular Formula:C₁₀H₁₃NO₃*ClH
Molecular Weight:231.679
Hs Code.:

Synonyms:Hydroxyamino-phenyl-acetic acid ethyl ester; hydrochloride

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Chemical Property of Hydroxyamino-phenyl-acetic acid ethyl ester; hydrochloride

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Technology Process of Hydroxyamino-phenyl-acetic acid ethyl ester; hydrochloride

There total 2 articles about Hydroxyamino-phenyl-acetic acid ethyl ester; hydrochloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

: 78437-22-6,110187-77-4
C₁₅H₁₅NO₄

: 78437-28-2
Hydroxyamino-phenyl-acetic acid ethyl ester; hydrochloride

: 1450-58-4
anti-furfuraldoxime

Guidance literature:: With hydroxylamine hydrochloride; In methanol; water; for 4h; Ambient temperature;
DOI:10.1248/cpb.34.3202

Reference yield:

: 2882-19-1,2216-90-2
ethyl 2-phenyl-2-bromoacetate

: 78437-28-2
Hydroxyamino-phenyl-acetic acid ethyl ester; hydrochloride

Guidance literature:: Multi-step reaction with 2 steps

1: 74 percent / Na / ethanol / 2 h / 40 °C

2: 94 percent / NH₂OH*HCl / methanol; H₂O / 4 h / Ambient temperature

With hydroxylamine hydrochloride; sodium; In methanol; ethanol; water;
DOI:10.1248/cpb.34.3202