3'-O-acetylthymmidin-5'-yl 5'-O-(9-phenylxanthen-9-yl)thymidin-3'-yl phosphorofluoridate

Base Information

Chemical Name:3'-O-acetylthymmidin-5'-yl 5'-O-(9-phenylxanthen-9-yl)thymidin-3'-yl phosphorofluoridate
CAS No.:119093-14-0
Molecular Formula:C₄₁H₄₀FN₄O₁₃P
Molecular Weight:846.76
Hs Code.:

Synonyms:3'-O-acetylthymmidin-5'-yl 5'-O-(9-phenylxanthen-9-yl)thymidin-3'-yl phosphorofluoridate

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Chemical Property of 3'-O-acetylthymmidin-5'-yl 5'-O-(9-phenylxanthen-9-yl)thymidin-3'-yl phosphorofluoridate

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Technology Process of 3'-O-acetylthymmidin-5'-yl 5'-O-(9-phenylxanthen-9-yl)thymidin-3'-yl phosphorofluoridate

There total 3 articles about 3'-O-acetylthymmidin-5'-yl 5'-O-(9-phenylxanthen-9-yl)thymidin-3'-yl phosphorofluoridate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.0%

: C₄₄H₄₃N₆O₁₃P

: 10364-94-0
1-benzoylimidazole

: 119093-14-0
3'-O-acetylthymmidin-5'-yl 5'-O-(9-phenylxanthen-9-yl)thymidin-3'-yl phosphorofluoridate

Guidance literature:: With benzoyl fluoride; In dichloromethane; for 1h; Ambient temperature;

Reference yield:

: 3'-O-acetylthymidine phosphorodifluoridate

: 69075-29-2
5'-O-pixylthymidine

: 119093-14-0
3'-O-acetylthymmidin-5'-yl 5'-O-(9-phenylxanthen-9-yl)thymidin-3'-yl phosphorofluoridate

Guidance literature:: With triethylamine; cesium fluoride; In acetonitrile; for 2h; Ambient temperature;

Reference yield:

: 21090-30-2
3'-O-acetylthymidine

: 143415-92-3
C₃₈H₄₈N₃O₇PSi

: 119093-14-0
3'-O-acetylthymmidin-5'-yl 5'-O-(9-phenylxanthen-9-yl)thymidin-3'-yl phosphorofluoridate

Guidance literature:: With 1H-tetrazole; fluorosulfonylchloride; Yield given. Multistep reaction; 1) MeCN, 20 min, 2) MeCN, a) -50 deg C to r.t., b) r.t., 1 h;