dimethyl-carbamic acid 4-[1-hydroxy-2-(4-nitro-phenoxy)-ethyl]-phenyl ester

Base Information

Chemical Name:dimethyl-carbamic acid 4-[1-hydroxy-2-(4-nitro-phenoxy)-ethyl]-phenyl ester
CAS No.:663180-35-6
Molecular Formula:C₁₇H₁₈N₂O₆
Molecular Weight:346.34
Hs Code.:

Synonyms:dimethyl-carbamic acid 4-[1-hydroxy-2-(4-nitro-phenoxy)-ethyl]-phenyl ester

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Chemical Property of dimethyl-carbamic acid 4-[1-hydroxy-2-(4-nitro-phenoxy)-ethyl]-phenyl ester

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Technology Process of dimethyl-carbamic acid 4-[1-hydroxy-2-(4-nitro-phenoxy)-ethyl]-phenyl ester

There total 7 articles about dimethyl-carbamic acid 4-[1-hydroxy-2-(4-nitro-phenoxy)-ethyl]-phenyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 84.0%

: 578730-12-8
dimethylcarbamic acid 4-[2-(4-nitrophenoxy)acetyl]phenyl ester

: 663180-35-6
dimethyl-carbamic acid 4-[1-hydroxy-2-(4-nitro-phenoxy)-ethyl]-phenyl ester

Guidance literature:: With sodium tetrahydroborate; In tetrahydrofuran; methanol; at 0 ℃; for 0.166667h;

Reference yield:

: 1798-11-4
4-nitrophenoxyacetic acid

: 663180-35-6
dimethyl-carbamic acid 4-[1-hydroxy-2-(4-nitro-phenoxy)-ethyl]-phenyl ester

Guidance literature:: Multi-step reaction with 6 steps

1.1: CH₂Cl₂ / 0.5 h / 20 °C

2.1: 7.10 g / CH₂Cl₂ / 12 h / 20 °C

3.1: n-BuLi / hexane; tetrahydrofuran / 0.5 h / -78 °C

3.2: 18 percent / hexane; tetrahydrofuran / 0.5 h / -78 °C

4.1: 250 mg / HCl / methanol; tetrahydrofuran; H₂O / 12 h / 20 °C

5.1: 201 mg / K₂CO₃ / dimethylformamide / 2 h / 20 °C

6.1: 84 percent / NaBH₄ / tetrahydrofuran; methanol / 0.17 h / 0 °C

With hydrogenchloride; sodium tetrahydroborate; n-butyllithium; potassium carbonate; In tetrahydrofuran; methanol; hexane; dichloromethane; water; N,N-dimethyl-formamide;

Reference yield:

: 98491-29-3
1-iodo-4-(methoxymethoxy)benzene

: 663180-35-6
dimethyl-carbamic acid 4-[1-hydroxy-2-(4-nitro-phenoxy)-ethyl]-phenyl ester

Guidance literature:: Multi-step reaction with 4 steps

1.1: n-BuLi / hexane; tetrahydrofuran / 0.5 h / -78 °C

1.2: 18 percent / hexane; tetrahydrofuran / 0.5 h / -78 °C

2.1: 250 mg / HCl / methanol; tetrahydrofuran; H₂O / 12 h / 20 °C

3.1: 201 mg / K₂CO₃ / dimethylformamide / 2 h / 20 °C

4.1: 84 percent / NaBH₄ / tetrahydrofuran; methanol / 0.17 h / 0 °C

With hydrogenchloride; sodium tetrahydroborate; n-butyllithium; potassium carbonate; In tetrahydrofuran; methanol; hexane; water; N,N-dimethyl-formamide;