2-bromo-N-(3,3-dimethyl-2-methylenebutyl)-4-fluoro-N-(4-methoxybenzyl)benzenesulfonamide

Base Information

Chemical Name:2-bromo-N-(3,3-dimethyl-2-methylenebutyl)-4-fluoro-N-(4-methoxybenzyl)benzenesulfonamide
CAS No.:1601490-04-3
Molecular Formula:C₂₁H₂₅BrFNO₃S
Molecular Weight:470.403
Hs Code.:

Synonyms:2-bromo-N-(3,3-dimethyl-2-methylenebutyl)-4-fluoro-N-(4-methoxybenzyl)benzenesulfonamide

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Chemical Property of 2-bromo-N-(3,3-dimethyl-2-methylenebutyl)-4-fluoro-N-(4-methoxybenzyl)benzenesulfonamide

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Technology Process of 2-bromo-N-(3,3-dimethyl-2-methylenebutyl)-4-fluoro-N-(4-methoxybenzyl)benzenesulfonamide

There total 4 articles about 2-bromo-N-(3,3-dimethyl-2-methylenebutyl)-4-fluoro-N-(4-methoxybenzyl)benzenesulfonamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 351003-45-7
2-bromo-4-fluorobenzene-1-sulfonyl chloride

: 1601490-04-3
2-bromo-N-(3,3-dimethyl-2-methylenebutyl)-4-fluoro-N-(4-methoxybenzyl)benzenesulfonamide

Guidance literature:: Multi-step reaction with 2 steps

1: pyridine / dichloromethane / 20 °C / Inert atmosphere

2: sodium iodide; caesium carbonate / N,N-dimethyl-formamide / 20 °C / Inert atmosphere

With pyridine; caesium carbonate; sodium iodide; In dichloromethane; N,N-dimethyl-formamide;
DOI:10.1016/j.tet.2014.03.038

Reference yield:

: 39497-64-8
3,3-dimethyl-2-methylenebutan-1-ol

: 1601490-04-3
2-bromo-N-(3,3-dimethyl-2-methylenebutyl)-4-fluoro-N-(4-methoxybenzyl)benzenesulfonamide

Guidance literature:: Multi-step reaction with 2 steps

1: phosphorus tribromide / diethyl ether / 0 - 20 °C / Inert atmosphere

2: sodium iodide; caesium carbonate / N,N-dimethyl-formamide / 20 °C / Inert atmosphere

With phosphorus tribromide; caesium carbonate; sodium iodide; In diethyl ether; N,N-dimethyl-formamide;
DOI:10.1016/j.tet.2014.03.038

Reference yield:

: 69060-18-0
3,3-dimethyl-2-methylenebutanal

: 1601490-04-3
2-bromo-N-(3,3-dimethyl-2-methylenebutyl)-4-fluoro-N-(4-methoxybenzyl)benzenesulfonamide

Guidance literature:: Multi-step reaction with 3 steps

1: sodium tetrahydroborate / diethyl ether; methanol / 0 - 20 °C / Inert atmosphere

2: phosphorus tribromide / diethyl ether / 0 - 20 °C / Inert atmosphere

3: sodium iodide; caesium carbonate / N,N-dimethyl-formamide / 20 °C / Inert atmosphere

With sodium tetrahydroborate; phosphorus tribromide; caesium carbonate; sodium iodide; In methanol; diethyl ether; N,N-dimethyl-formamide;
DOI:10.1016/j.tet.2014.03.038