2-cyclohexyl-1,1-diphenylethylhydroperoxide

Base Information

Chemical Name:2-cyclohexyl-1,1-diphenylethylhydroperoxide
CAS No.:1454681-01-6
Molecular Formula:C₂₀H₂₄O₂
Molecular Weight:296.409
Hs Code.:

Synonyms:2-cyclohexyl-1,1-diphenylethylhydroperoxide

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Chemical Property of 2-cyclohexyl-1,1-diphenylethylhydroperoxide

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Technology Process of 2-cyclohexyl-1,1-diphenylethylhydroperoxide

There total 3 articles about 2-cyclohexyl-1,1-diphenylethylhydroperoxide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

: 1454679-72-1
2-cyclohexyl-1,1-diphenylethanol

: 1454681-01-6
2-cyclohexyl-1,1-diphenylethylhydroperoxide

Guidance literature:: With sulfuric acid; dihydrogen peroxide; In tetrahydrofuran; water; at 0 - 60 ℃; for 24h;
DOI:10.3762/bjoc.9.138

Reference yield:

: 5452-75-5
ethyl 2-cyclohexylacetate

: 1454681-01-6
2-cyclohexyl-1,1-diphenylethylhydroperoxide

Guidance literature:: Multi-step reaction with 2 steps

1: diethyl ether / -78 - 20 °C

2: dihydrogen peroxide; sulfuric acid / tetrahydrofuran; water / 24 h / 0 - 60 °C

With sulfuric acid; dihydrogen peroxide; In tetrahydrofuran; diethyl ether; water;
DOI:10.3762/bjoc.9.138

Reference yield:

: 100-58-3
phenylmagnesium bromide

: 1454681-01-6
2-cyclohexyl-1,1-diphenylethylhydroperoxide

Guidance literature:: Multi-step reaction with 2 steps

1: diethyl ether / -78 - 20 °C

2: dihydrogen peroxide; sulfuric acid / tetrahydrofuran; water / 24 h / 0 - 60 °C

With sulfuric acid; dihydrogen peroxide; In tetrahydrofuran; diethyl ether; water;
DOI:10.3762/bjoc.9.138