C₂₉H₄₆O₂Si

Base Information

Chemical Name:C₂₉H₄₆O₂Si
CAS No.:943898-01-9
Molecular Formula:C₂₉H₄₆O₂Si
Molecular Weight:454.769
Hs Code.:

C<sub>29</sub>H<sub>46</sub>O<sub>2</sub>Si

Synonyms:C₂₉H₄₆O₂Si

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Chemical Property of C₂₉H₄₆O₂Si

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Technology Process of C₂₉H₄₆O₂Si

There total 7 articles about C₂₉H₄₆O₂Si which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 943898-00-8
C₃₉H₅₃O₄SiN

: 943898-01-9
C₂₉H₄₆O₂Si

Guidance literature:: With lithium borohydride; In diethyl ether; ethanol; at 0 ℃; for 2h;
DOI:10.1021/ol070517g

Reference yield:

: 633323-32-7
C₂₉H₄₄SiO₃

: 943898-01-9
C₂₉H₄₆O₂Si

Guidance literature:: Multi-step reaction with 5 steps

1.1: 90 percent / lithium hydroxide monohydrate / tetrahydrofuran; methanol; H₂O / 5 h / 20 °C

2.1: oxalyl chloride / benzene; dimethylformamide / 4 h / 20 °C

3.1: 92 percent / butyllithium / tetrahydrofuran; hexane / -78 °C

4.1: sodium bis(trimethylsilyl)amide / tetrahydrofuran / 0.5 h / -78 °C

4.2: 78 percent / tetrahydrofuran / 5 h / -78 °C

5.1: 90 percent / lithium borohydride / diethyl ether; ethanol / 2 h / 0 °C

With lithium hydroxide; lithium borohydride; n-butyllithium; oxalyl dichloride; sodium hexamethyldisilazane; In tetrahydrofuran; methanol; diethyl ether; ethanol; hexane; water; N,N-dimethyl-formamide; benzene;
DOI:10.1021/ol070517g

Reference yield:

: 943897-99-2
C₃₈H₅₁O₄SiN

: 943898-01-9
C₂₉H₄₆O₂Si

Guidance literature:: Multi-step reaction with 2 steps

1.1: sodium bis(trimethylsilyl)amide / tetrahydrofuran / 0.5 h / -78 °C

1.2: 78 percent / tetrahydrofuran / 5 h / -78 °C

2.1: 90 percent / lithium borohydride / diethyl ether; ethanol / 2 h / 0 °C

With lithium borohydride; sodium hexamethyldisilazane; In tetrahydrofuran; diethyl ether; ethanol;
DOI:10.1021/ol070517g