4-[4-acetyl-3-[3-[3-(4-acetyl-3-hydroxy-2-propylphenoxy)propoxy]propoxy]-2-propylphenoxy]butanoic acid ethyl ester

Base Information

• Chemical Name: 4-[4-acetyl-3-[3-[3-(4-acetyl-3-hydroxy-2-propylphenoxy)propoxy]propoxy]-2-propylphenoxy]butanoic acid ethyl ester
• CAS No.: 88420-16-0
• Molecular Formula: C₃₄H₄₈O₉
• Molecular Weight: 600.75

Synonyms:4-[4-acetyl-3-[3-[3-(4-acetyl-3-hydroxy-2-propylphenoxy)propoxy]propoxy]-2-propylphenoxy]butanoic acid ethyl ester

Chemical Property of 4-[4-acetyl-3-[3-[3-(4-acetyl-3-hydroxy-2-propylphenoxy)propoxy]propoxy]-2-propylphenoxy]butanoic acid ethyl ester

Chemical Property:

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Technology Process of 4-[4-acetyl-3-[3-[3-(4-acetyl-3-hydroxy-2-propylphenoxy)propoxy]propoxy]-2-propylphenoxy]butanoic acid ethyl ester

There total 4 articles about 4-[4-acetyl-3-[3-[3-(4-acetyl-3-hydroxy-2-propylphenoxy)propoxy]propoxy]-2-propylphenoxy]butanoic acid ethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

1-(2,4-dihydroxy-3-propylphenyl)ethanone (40786-69-4) + 4-[4-acetyl-3-[3-(3-bromopropoxy)propoxy]-2-propylphenoxy]butanoic acid ethyl ester (88420-47-7) → 4-[4-acetyl-3-[3-[3-(4-acetyl-3-hydroxy-2-propylphenoxy)propoxy]propoxy]-2-propylphenoxy]butanoic acid ethyl ester (88420-16-0)

Guidance literature:

With potassium carbonate; In N,N-dimethyl-formamide; acetone; for 17h; Heating;

DOI:10.1021/jm00384a029

Reference yield:

1-(2,4-dihydroxy-3-propylphenyl)ethanone (40786-69-4) → 4-[4-acetyl-3-[3-[3-(4-acetyl-3-hydroxy-2-propylphenoxy)propoxy]propoxy]-2-propylphenoxy]butanoic acid ethyl ester (88420-16-0)

Guidance literature:

Multi-step reaction with 3 steps

1: 54 percent / K₂CO₃ / dimethylformamide / 12 h / 75 °C

2: K₂CO₃ / acetone / 77 h / Heating

3: 82 percent / K₂CO₃ / acetone; dimethylformamide / 17 h / Heating

With potassium carbonate; In N,N-dimethyl-formamide; acetone;

DOI:10.1021/jm00384a029

Reference yield:

Ethyl 4-bromobutyrate (2969-81-5) → 4-[4-acetyl-3-[3-[3-(4-acetyl-3-hydroxy-2-propylphenoxy)propoxy]propoxy]-2-propylphenoxy]butanoic acid ethyl ester (88420-16-0)

Guidance literature:

Multi-step reaction with 3 steps

1: 54 percent / K₂CO₃ / dimethylformamide / 12 h / 75 °C

2: K₂CO₃ / acetone / 77 h / Heating

3: 82 percent / K₂CO₃ / acetone; dimethylformamide / 17 h / Heating

With potassium carbonate; In N,N-dimethyl-formamide; acetone;

DOI:10.1021/jm00384a029

upstream raw materials:

1-(2,4-dihydroxy-3-propylphenyl)ethanone

4-[4-acetyl-3-[3-(3-bromopropoxy)propoxy]-2-propylphenoxy]butanoic acid ethyl ester

Ethyl 4-bromobutyrate

4-(4-acetyl-3-hydroxy-2-propylphenoxy)-butanoic acid ethyl ester

Downstream raw materials:

4-[4-acetyl-3-[3-[3-(4-acetyl-3-hydroxy-2-propylphenoxy)propoxy]propoxy]-2-propylphenoxy]butanoic acid

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