3-hydroxy-3-methyl-4-oxo-4-phenylbutyl-3-(2,2-diphenylcyclopropyl)-2,2-dimethyl-3-oxopropanoate

Base Information

Chemical Name:3-hydroxy-3-methyl-4-oxo-4-phenylbutyl-3-(2,2-diphenylcyclopropyl)-2,2-dimethyl-3-oxopropanoate
CAS No.:936355-53-2
Molecular Formula:C₃₁H₃₂O₅
Molecular Weight:484.592
Hs Code.:

Synonyms:3-hydroxy-3-methyl-4-oxo-4-phenylbutyl-3-(2,2-diphenylcyclopropyl)-2,2-dimethyl-3-oxopropanoate

Suppliers and Price of 3-hydroxy-3-methyl-4-oxo-4-phenylbutyl-3-(2,2-diphenylcyclopropyl)-2,2-dimethyl-3-oxopropanoate

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of 3-hydroxy-3-methyl-4-oxo-4-phenylbutyl-3-(2,2-diphenylcyclopropyl)-2,2-dimethyl-3-oxopropanoate

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of 3-hydroxy-3-methyl-4-oxo-4-phenylbutyl-3-(2,2-diphenylcyclopropyl)-2,2-dimethyl-3-oxopropanoate

There total 5 articles about 3-hydroxy-3-methyl-4-oxo-4-phenylbutyl-3-(2,2-diphenylcyclopropyl)-2,2-dimethyl-3-oxopropanoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 43.0%

: 936355-48-5
2,4-dihydroxy-2-methyl-1-phenylbutan-1-one

: 936355-51-0
3-(2,2-diphenylcyclopropyl)-2,2-dimethyl-3-oxopropanoic acid

: 936355-53-2
3-hydroxy-3-methyl-4-oxo-4-phenylbutyl-3-(2,2-diphenylcyclopropyl)-2,2-dimethyl-3-oxopropanoate

Guidance literature:: With dmap; dicyclohexyl-carbodiimide; In dichloromethane;
DOI:10.1021/ol070593j

Reference yield:

: 936355-50-9
methyl 3-(2,2-diphenylcyclopropyl)-2,2-dimethyl-3-oxopropanoate

: 936355-53-2
3-hydroxy-3-methyl-4-oxo-4-phenylbutyl-3-(2,2-diphenylcyclopropyl)-2,2-dimethyl-3-oxopropanoate

Guidance literature:: Multi-step reaction with 2 steps

1: 95 percent / lithium hydroxide / ethanol; H₂O / 20 °C

2: 43 percent / DCC; DMAP / CH₂Cl₂

With dmap; lithium hydroxide; dicyclohexyl-carbodiimide; In ethanol; dichloromethane; water;
DOI:10.1021/ol070593j

Reference yield:

: 936355-47-4
4-(tert-butyldimethylsilyloxy)2-hydroxy-2-methyl-1-phenylbutan-1-one

: 936355-53-2
3-hydroxy-3-methyl-4-oxo-4-phenylbutyl-3-(2,2-diphenylcyclopropyl)-2,2-dimethyl-3-oxopropanoate

Guidance literature:: Multi-step reaction with 2 steps

1: tetrabutylammonium fluoride / tetrahydrofuran / 0.33 h / 20 °C

2: 43 percent / DCC; DMAP / CH₂Cl₂

With dmap; tetrabutyl ammonium fluoride; dicyclohexyl-carbodiimide; In tetrahydrofuran; dichloromethane;
DOI:10.1021/ol070593j