C₂₆H₂₁BrN₆O₄S

Base Information

Chemical Name:C₂₆H₂₁BrN₆O₄S
CAS No.:1315476-19-7
Molecular Formula:C₂₆H₂₁BrN₆O₄S
Molecular Weight:593.461
Hs Code.:

C<sub>26</sub>H<sub>21</sub>BrN<sub>6</sub>O<sub>4</sub>S

Synonyms:C₂₆H₂₁BrN₆O₄S

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Chemical Property of C₂₆H₂₁BrN₆O₄S

Chemical Property:

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Technology Process of C₂₆H₂₁BrN₆O₄S

There total 19 articles about C₂₆H₂₁BrN₆O₄S which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 45.0%

: 590385-73-2
(+)-5-(toluene-4-sulfonyl)-3,5,7,8,9,10-hexahydro-2H-triazaacephenanthrylen-6-one-8-(hydroxymethyl)-10-spiro-4'-(2'-bromo)cyclohexa-2',5'-dien-1'-one

: 1315476-19-7
C₂₆H₂₁BrN₆O₄S

Guidance literature:: With diphenyl phosphoryl azide; triphenylphosphine; diethylazodicarboxylate; In toluene; at 0 - 20 ℃; for 7h; Inert atmosphere;
DOI:10.1039/c1ob05058c

Reference yield:

: 55149-84-3
2-nitroveratraldehyde

: 1315476-19-7
C₂₆H₂₁BrN₆O₄S

Guidance literature:: Multi-step reaction with 11 steps

1: potassium hydroxide / ethanol; N,N-dimethyl-formamide / 1.25 h / -2 °C

2: palladium on carbon; formic acid; ammonium formate / methanol / 1 h

3: 2 h / 0 °C

4: lithium aluminium tetrahydride / tetrahydrofuran / 2.5 h / Reflux

5: diphenyl phosphoryl azide; triphenylphosphine; diethylazodicarboxylate / toluene / 9 h

6: potassium tert-butylate / tetrahydrofuran / 6 h / 0 °C

7: 1,1,1,3',3',3'-hexafluoro-propanol; trimethylsilyl trifluoromethanesulfonate; bis-[(trifluoroacetoxy)iodo]benzene / water / 1 h / 0 °C

8: hydrogenchloride / methanol / 36 h / 20 °C

9: bis-[(trifluoroacetoxy)iodo]benzene / 2,2,2-trifluoroethanol / 7 h / 20 °C

10: boron trifluoride diethyl etherate / dichloromethane / 7 h / 0 - 20 °C

11: diphenyl phosphoryl azide; triphenylphosphine; diethylazodicarboxylate / toluene / 7 h / 0 - 20 °C / Inert atmosphere

With hydrogenchloride; lithium aluminium tetrahydride; formic acid; 1,1,1,3',3',3'-hexafluoro-propanol; trimethylsilyl trifluoromethanesulfonate; diphenyl phosphoryl azide; palladium on carbon; boron trifluoride diethyl etherate; potassium tert-butylate; ammonium formate; triphenylphosphine; bis-[(trifluoroacetoxy)iodo]benzene; potassium hydroxide; diethylazodicarboxylate; In tetrahydrofuran; methanol; ethanol; dichloromethane; 2,2,2-trifluoroethanol; water; N,N-dimethyl-formamide; toluene; 5: Mitsunobu reaction / 11: Mitsunobu reaction;
DOI:10.1039/c1ob05058c

Reference yield:

: 31165-13-6
6,7-dimethoxy-1H-indole

: 1315476-19-7
C₂₆H₂₁BrN₆O₄S

Guidance literature:: Multi-step reaction with 9 steps

1: 2 h / 0 °C

2: lithium aluminium tetrahydride / tetrahydrofuran / 2.5 h / Reflux

3: diphenyl phosphoryl azide; triphenylphosphine; diethylazodicarboxylate / toluene / 9 h

4: potassium tert-butylate / tetrahydrofuran / 6 h / 0 °C

5: 1,1,1,3',3',3'-hexafluoro-propanol; trimethylsilyl trifluoromethanesulfonate; bis-[(trifluoroacetoxy)iodo]benzene / water / 1 h / 0 °C

6: hydrogenchloride / methanol / 36 h / 20 °C

7: bis-[(trifluoroacetoxy)iodo]benzene / 2,2,2-trifluoroethanol / 7 h / 20 °C

8: boron trifluoride diethyl etherate / dichloromethane / 7 h / 0 - 20 °C

9: diphenyl phosphoryl azide; triphenylphosphine; diethylazodicarboxylate / toluene / 7 h / 0 - 20 °C / Inert atmosphere

With hydrogenchloride; lithium aluminium tetrahydride; 1,1,1,3',3',3'-hexafluoro-propanol; trimethylsilyl trifluoromethanesulfonate; diphenyl phosphoryl azide; boron trifluoride diethyl etherate; potassium tert-butylate; triphenylphosphine; bis-[(trifluoroacetoxy)iodo]benzene; diethylazodicarboxylate; In tetrahydrofuran; methanol; dichloromethane; 2,2,2-trifluoroethanol; water; toluene; 3: Mitsunobu reaction / 9: Mitsunobu reaction;
DOI:10.1039/c1ob05058c