(1-{1-[1-Chloro-1-methoxy-meth-(Z)-ylidene]-propyl}-2-ethyl-3-methoxy-1H-1λ⁵-phosphiren-1-ylidene)-(2,4,6-tri-tert-butyl-phenyl)-amine

Base Information

• Chemical Name: (1-{1-[1-Chloro-1-methoxy-meth-(Z)-ylidene]-propyl}-2-ethyl-3-methoxy-1H-1λ⁵-phosphiren-1-ylidene)-(2,4,6-tri-tert-butyl-phenyl)-amine
• CAS No.: 174970-96-8
• Molecular Formula: C₂₈H₄₅ClNO₂P
• Molecular Weight: 494.098

Synonyms:(1-{1-[1-Chloro-1-methoxy-meth-(Z)-ylidene]-propyl}-2-ethyl-3-methoxy-1H-1λ⁵-phosphiren-1-ylidene)-(2,4,6-tri-tert-butyl-phenyl)-amine

Chemical Property of (1-{1-[1-Chloro-1-methoxy-meth-(Z)-ylidene]-propyl}-2-ethyl-3-methoxy-1H-1λ⁵-phosphiren-1-ylidene)-(2,4,6-tri-tert-butyl-phenyl)-amine

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Technology Process of (1-{1-[1-Chloro-1-methoxy-meth-(Z)-ylidene]-propyl}-2-ethyl-3-methoxy-1H-1λ⁵-phosphiren-1-ylidene)-(2,4,6-tri-tert-butyl-phenyl)-amine

There total 3 articles about (1-{1-[1-Chloro-1-methoxy-meth-(Z)-ylidene]-propyl}-2-ethyl-3-methoxy-1H-1λ⁵-phosphiren-1-ylidene)-(2,4,6-tri-tert-butyl-phenyl)-amine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

ethylmethoxyacetylene (13279-94-2) + C23H37ClNOP (174970-85-5) → (1-{1-[1-Chloro-1-methoxy-meth-(E)-ylidene]-propyl}-2-ethyl-3-methoxy-1H-1λ5-phosphiren-1-ylidene)-(2,4,6-tri-tert-butyl-phenyl)-amine + (1-{1-[1-Chloro-1-methoxy-meth-(Z)-ylidene]-propyl}-2-ethyl-3-methoxy-1H-1λ5-phosphiren-1-ylidene)-(2,4,6-tri-tert-butyl-phenyl)-amine (174970-96-8)

Guidance literature:

In dichloromethane; for 12h;

Reference yield:

ethylmethoxyacetylene (13279-94-2) → (1-{1-[1-Chloro-1-methoxy-meth-(Z)-ylidene]-propyl}-2-ethyl-3-methoxy-1H-1λ5-phosphiren-1-ylidene)-(2,4,6-tri-tert-butyl-phenyl)-amine (174970-96-8)

Guidance literature:

Multi-step reaction with 2 steps

1: 92 percent / CH₂Cl₂ / 0.42 h / 20 °C

2: 90 percent / CH₂Cl₂ / 12 h

In dichloromethane;

Reference yield:

P-chloro-N-(2,4,6-tri-tert-butylphenyl)-λ3-iminophosphine (117688-09-2,124775-15-1) → (1-{1-[1-Chloro-1-methoxy-meth-(Z)-ylidene]-propyl}-2-ethyl-3-methoxy-1H-1λ5-phosphiren-1-ylidene)-(2,4,6-tri-tert-butyl-phenyl)-amine (174970-96-8)

Guidance literature:

Multi-step reaction with 2 steps

1: 92 percent / CH₂Cl₂ / 0.42 h / 20 °C

2: 90 percent / CH₂Cl₂ / 12 h

In dichloromethane;

upstream raw materials:

ethylmethoxyacetylene

C₂₃H₃₇ClNOP

P-chloro-N-(2,4,6-tri-tert-butylphenyl)-λ³-iminophosphine

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