2-methylbenzyl tosylate

Base Information

Chemical Name:2-methylbenzyl tosylate
CAS No.:41194-46-1
Molecular Formula:C₁₅H₁₆O₃S
Molecular Weight:276.356
Hs Code.:

Synonyms:2-methylbenzyl tosylate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2-methylbenzyl tosylate

Chemical Property:

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Technology Process of 2-methylbenzyl tosylate

There total 1 articles about 2-methylbenzyl tosylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 89-95-2
2-methyl-benzyl alcohol

: 98-59-9
p-toluenesulfonyl chloride

: 41194-46-1
2-methylbenzyl tosylate

Guidance literature:: With sodium hydride; Yield given. Multistep reaction; 1.) Et₂O, a) reflux, 3 h, b) 20 deg C, 20 h, 2.) Et₂O, a) -20 deg C, 2 h, b) 20 deg C, 2 h;
DOI:10.1002/ijch.199600022

Reference yield: 99.0%

: 5720-07-0
4-methoxyphenylboronic acid

: 41194-46-1
2-methylbenzyl tosylate

: 53039-52-4
1-methyl-2-(4-methoxybenzyl) benzene

Guidance literature:: With NHC-Pd(II)-Im; sodium hydroxide; In tetrahydrofuran; at 100 ℃; for 12h; Inert atmosphere; Sealed tube;
DOI:10.1039/c4ob02675f

Reference yield: 94.0%

: 41194-46-1
2-methylbenzyl tosylate

: 98-80-6
phenylboronic acid

: 713-36-0
2-benzyltoluene

Guidance literature:: With NHC-Pd(II)-Im; sodium hydroxide; In tetrahydrofuran; at 100 ℃; for 12h; Inert atmosphere; Sealed tube;
DOI:10.1039/c4ob02675f