trans-4-{4-(2,3-epoxypropoxy)phenyl}cyclohexyl 4-(2,3-epoxypropoxy)benzoate

Base Information

Chemical Name:trans-4-{4-(2,3-epoxypropoxy)phenyl}cyclohexyl 4-(2,3-epoxypropoxy)benzoate
CAS No.:1268813-67-7
Molecular Formula:C₂₅H₂₈O₆
Molecular Weight:424.494
Hs Code.:

Synonyms:trans-4-{4-(2,3-epoxypropoxy)phenyl}cyclohexyl 4-(2,3-epoxypropoxy)benzoate

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Chemical Property of trans-4-{4-(2,3-epoxypropoxy)phenyl}cyclohexyl 4-(2,3-epoxypropoxy)benzoate

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Technology Process of trans-4-{4-(2,3-epoxypropoxy)phenyl}cyclohexyl 4-(2,3-epoxypropoxy)benzoate

There total 2 articles about trans-4-{4-(2,3-epoxypropoxy)phenyl}cyclohexyl 4-(2,3-epoxypropoxy)benzoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 84.0%

: 1268813-66-6
C₁₉H₂₀O₄

: 106-89-8,24969-06-0,13403-37-7
epichlorohydrin

: 1268813-67-7
trans-4-{4-(2,3-epoxypropoxy)phenyl}cyclohexyl 4-(2,3-epoxypropoxy)benzoate

Guidance literature:: C₁₉H₂₀O₄; epichlorohydrin; With tetrabutylammomium bromide; at 70 ℃; for 5h;

With sodium hydroxide; In water; at 18 ℃; for 2h; Product distribution / selectivity;

Reference yield:

: 65132-43-6
trans-4,4'-dihydroxy-cyclohexylbenzene

: 99-96-7
4-hydroxy-benzoic acid

: 1268813-67-7
trans-4-{4-(2,3-epoxypropoxy)phenyl}cyclohexyl 4-(2,3-epoxypropoxy)benzoate

Guidance literature:: Multi-step reaction with 2 steps

1.1: toluene-4-sulfonic acid / chlorobenzene / 16 h / Reflux

2.1: tetrabutylammomium bromide / 5 h / 70 °C

2.2: 2 h / 18 °C

With tetrabutylammomium bromide; toluene-4-sulfonic acid; In chlorobenzene;