Ir2(μ-PPh2)2(CO)2(PPh3)2

Base Information

Chemical Name:Ir2(μ-PPh2)2(CO)2(PPh3)2
CAS No.:39732-63-3
Molecular Formula:C₆₂H₅₀Ir₂O₂P₄
Molecular Weight:1335.41
Hs Code.:

Synonyms:Ir2(μ-PPh2)2(CO)2(PPh3)2

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Chemical Property of Ir2(μ-PPh2)2(CO)2(PPh3)2

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Technology Process of Ir2(μ-PPh2)2(CO)2(PPh3)2

There total 9 articles about Ir2(μ-PPh2)2(CO)2(PPh3)2 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 59246-46-7,14871-41-1,15318-31-7
bis(triphenylphosphine)carbonyliridium(I) chloride

: 829-85-6
diphenylphosphane

: 39732-63-3
[Rh(μ-PPh2)(CO)PPh3]2

Guidance literature:: With n-butyllithium; In tetrahydrofuran; Ph2PH was treated with n-BuLi under N2; prepd. soln. was added to soln.of Ir complex under N2, react. time 1 h; filtration, washing with THF, drying in vac.;

Reference yield: 49.0%

: 33541-67-2
carbonylhydridotris(triphenylphosphine)iridium(I)

: 39732-63-3
Ir2(μ-PPh2)2(CO)2(PPh3)2

: 85655-33-0
hydridobis(triphenylphosphine)bis(acetato)iridium

Guidance literature:: In N,N-dimethyl-formamide; refluxed for 4 h; cooled, filtered off, washed with EtOH and Et2O, elem. anal., EtOH added to the mother liquor, left to stand for 40 h at room temp., pptn. washed with EtOH and hexane, recrystd. from benzene and hexane, elem. anal.;

Reference yield: 49.0%

: 18660-46-3,18660-47-4,16924-01-9
[Ir(H)₃(triphenylphosphine)₃]

: 39732-63-3
Ir2(μ-PPh2)2(CO)2(PPh3)2

: 85655-33-0
hydridobis(triphenylphosphine)bis(acetato)iridium

Guidance literature:: In N,N-dimethyl-formamide; refluxed for 4 h; cooled, filtered off, washed with EtOH and Et2O, EtOH added to the mother liquor, left to stand for 40 h at room temp., pptn. washed with EtOH and hexane, recrystd. from benzene and hexane, elem. anal.;