[ZnCl₂(bis(3,5-bis(trifluoromethyl)phenyl)acenaphthenequinonediimine)]

Base Information

Chemical Name:[ZnCl₂(bis(3,5-bis(trifluoromethyl)phenyl)acenaphthenequinonediimine)]
CAS No.:798567-18-7
Molecular Formula:C₂₈H₁₂Cl₂F₁₂N₂Zn
Molecular Weight:740.694
Hs Code.:

[ZnCl<sub>2</sub>(bis(3,5-bis(trifluoromethyl)phenyl)acenaphthenequinonediimine)]

Synonyms:[ZnCl₂(bis(3,5-bis(trifluoromethyl)phenyl)acenaphthenequinonediimine)]

Suppliers and Price of [ZnCl₂(bis(3,5-bis(trifluoromethyl)phenyl)acenaphthenequinonediimine)]

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Chemical Property of [ZnCl₂(bis(3,5-bis(trifluoromethyl)phenyl)acenaphthenequinonediimine)]

Chemical Property:

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Technology Process of [ZnCl₂(bis(3,5-bis(trifluoromethyl)phenyl)acenaphthenequinonediimine)]

There total 1 articles about [ZnCl₂(bis(3,5-bis(trifluoromethyl)phenyl)acenaphthenequinonediimine)] which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 328-74-5
3,5-Bis-(trifluoromethyl)aniline

: 7646-85-7,24359-56-6
zinc(II) chloride

: 82-86-0
acenaphthene quinone

: 798567-18-7
[ZnCl₂(bis(3,5-bis(trifluoromethyl)phenyl)acenaphthenequinonediimine)]

Guidance literature:: In acetic acid; toluene; ZnCl2 and acenaphthenequinone were suspended in acetic acid and toluene and heated to 50-60°C, aniline was added and heated at reflux for45 min; react. mixt. was filtered hot, ppt. was washed with Et2O and dried in vacuo;
DOI:10.1021/om020147u

Reference yield: 70.0%

: 798567-18-7
[ZnCl₂(bis(3,5-bis(trifluoromethyl)phenyl)acenaphthenequinonediimine)]

: 4-amino-4'-(diphenylphosphanyl)biphenyl

: 1-[4-(4-diphenylphosphanylphenyl)phenylimino]-2-[3,5-bis(trifluoromethyl)phenylimino]acenaphthene

: 1,2-bis[4-(4-diphenylphosphanylphenyl)phenylimino]acenaphthene

Guidance literature:: [ZnCl₂(bis(3,5-bis(trifluoromethyl)phenyl)acenaphthenequinonediimine)]; 4-amino-4'-(diphenylphosphanyl)biphenyl; In methanol; at 45 ℃; for 21h; Schlenk technique; Inert atmosphere; Sealed tube;

With sodium oxalate; In dichloromethane; water; Schlenk technique; Inert atmosphere; Sealed tube;
DOI:10.1016/j.poly.2015.03.008

Reference yield: 65.0%

: 798567-18-7
[ZnCl₂(bis(3,5-bis(trifluoromethyl)phenyl)acenaphthenequinonediimine)]

: 583-52-8
potassium oxalate

: 226071-21-2
N,N'-bis(bis(3,5-trifluoromethyl)phenyl)acenaphthenequinonediimine

: 547-68-2
zinc(II) oxalate

Guidance literature:: In dichloromethane; water; Zn complex was suspended in CH2Cl2 and soln. potassium oxalate in water was added, shaked for 5 min;
DOI:10.1021/om020147u