2,3,4-tri-O-benzoyl-β-D-glucopyranosylamine hydrochloride

Base Information

• Chemical Name: 2,3,4-tri-O-benzoyl-β-D-glucopyranosylamine hydrochloride
• CAS No.: 144336-41-4
• Molecular Formula: C₂₇H₂₅NO₈*ClH
• Molecular Weight: 527.958
• Mol file: 144336-41-4.mol

Synonyms:2,3,4-tri-O-benzoyl-β-D-glucopyranosylamine hydrochloride

Chemical Property of 2,3,4-tri-O-benzoyl-β-D-glucopyranosylamine hydrochloride

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 2,3,4-tri-O-benzoyl-β-D-glucopyranosylamine hydrochloride

There total 1 articles about 2,3,4-tri-O-benzoyl-β-D-glucopyranosylamine hydrochloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

2,3,4-tri-O-benzoyl-N-(2,2-diethoxycarbonylvinyl)-6-O-trityl-β-D-glucopyranosylamine (144310-53-2) → 2,3,4-tri-O-benzoyl-β-D-glucopyranosylamine hydrochloride (144336-41-4)

Guidance literature:

With chlorine; In dichloromethane;

DOI:10.1016/S0040-4020(01)88231-4

Reference yield: 64.0%

thiophosgene (463-71-8) + 2,3,4-tri-O-benzoyl-β-D-glucopyranosylamine hydrochloride (144336-41-4) → 2,3,4-tri-O-benzoyl-β-D-glucopyranosyl isothiocyanate (144219-37-4)

Guidance literature:

With calcium carbonate; In dichloromethane; water; for 48h;

DOI:10.1016/S0040-4020(01)88231-4

Reference yield:

2,3,4-tri-O-benzoyl-β-D-glucopyranosylamine hydrochloride (144336-41-4) → 2-(2',3',4'-tri-O-benzoyl-β-D-glucopyranosyl)amino-2-thiazoline (144219-43-2)

Guidance literature:

Multi-step reaction with 2 steps

1: 64 percent / CaCO₃ / CH₂Cl₂; H₂O / 48 h

2: 97 percent / diethyl ether / 12 h / Ambient temperature

With calcium carbonate; In diethyl ether; dichloromethane; water;

DOI:10.1016/S0040-4020(01)88231-4

upstream raw materials:

2,3,4-tri-O-benzoyl-N-(2,2-diethoxycarbonylvinyl)-6-O-trityl-β-D-glucopyranosylamine

Downstream raw materials:

2,3,4-tri-O-benzoyl-β-D-glucopyranosyl isothiocyanate

2-(2',3',4'-tri-O-benzoyl-β-D-glucopyranosyl)amino-2-thiazoline

5-methyl-1-(2',3',4'-tri-O-benzoyl-β-D-glucopyranosyl)-4-imidazoline-2-thione

N-phenacyl-N-(2,3,4-tri-O-benzoyl-β-D-glucopyranosyl)thiourea