(4S,5R)-5-((R)-1,2-Dihydroxy-ethyl)-2,2-dimethyl-[1,3]dioxolane-4-carboxylic acid benzyloxy-amide

Base Information

Chemical Name:(4S,5R)-5-((R)-1,2-Dihydroxy-ethyl)-2,2-dimethyl-[1,3]dioxolane-4-carboxylic acid benzyloxy-amide
CAS No.:176755-16-1
Molecular Formula:C₁₅H₂₁NO₆
Molecular Weight:311.335
Hs Code.:

Synonyms:(4S,5R)-5-((R)-1,2-Dihydroxy-ethyl)-2,2-dimethyl-[1,3]dioxolane-4-carboxylic acid benzyloxy-amide

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Chemical Property of (4S,5R)-5-((R)-1,2-Dihydroxy-ethyl)-2,2-dimethyl-[1,3]dioxolane-4-carboxylic acid benzyloxy-amide

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Technology Process of (4S,5R)-5-((R)-1,2-Dihydroxy-ethyl)-2,2-dimethyl-[1,3]dioxolane-4-carboxylic acid benzyloxy-amide

There total 6 articles about (4S,5R)-5-((R)-1,2-Dihydroxy-ethyl)-2,2-dimethyl-[1,3]dioxolane-4-carboxylic acid benzyloxy-amide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

: 176755-14-9
(4R,5S,4'R)-2,2,2',2'-Tetramethyl-[4,4']bi[[1,3]dioxolanyl]-5-carboxylic acid benzyloxy-amide

: 176755-16-1
(4S,5R)-5-((R)-1,2-Dihydroxy-ethyl)-2,2-dimethyl-[1,3]dioxolane-4-carboxylic acid benzyloxy-amide

Guidance literature:: In acetic acid; at 20 ℃; for 16h;
DOI:10.1016/0040-4039(96)00254-7

Reference yield:

: 10323-20-3
D-Arabinose

: 176755-16-1
(4S,5R)-5-((R)-1,2-Dihydroxy-ethyl)-2,2-dimethyl-[1,3]dioxolane-4-carboxylic acid benzyloxy-amide

Guidance literature:: Multi-step reaction with 6 steps

1: 81 percent / HCl, ZnCl₂

2: 99 percent / CuSO₄, H₂SO₄

3: 66 percent / HgO, HgCl₂ / acetone; H₂O

4: 65 percent / AgNO₃, NaOH / methanol

5: 85 percent / HNEt₂, DCC / CH₂Cl₂

6: 88 percent / aq. acetic acid / 16 h / 20 °C

With hydrogenchloride; sodium hydroxide; sulfuric acid; silver nitrate; copper(II) sulfate; diethylamine; dicyclohexyl-carbodiimide; mercury dichloride; mercury(II) oxide; zinc(II) chloride; In methanol; dichloromethane; water; acetic acid; acetone;
DOI:10.1016/0040-4039(96)00254-7

Reference yield:

: 30694-81-6
O²,O³;O⁴,O⁵-diisopropyliden-D-arabinonic acid

: 176755-16-1
(4S,5R)-5-((R)-1,2-Dihydroxy-ethyl)-2,2-dimethyl-[1,3]dioxolane-4-carboxylic acid benzyloxy-amide

Guidance literature:: Multi-step reaction with 2 steps

1: 85 percent / HNEt₂, DCC / CH₂Cl₂

2: 88 percent / aq. acetic acid / 16 h / 20 °C

With diethylamine; dicyclohexyl-carbodiimide; In dichloromethane; acetic acid;
DOI:10.1016/0040-4039(96)00254-7