1,6-di-O-(tert-butyldiphenylsilyl)-2,5-di-O-(4-methoxybenzyl)-D-mannitol

Base Information Edit

Chemical Name:1,6-di-O-(tert-butyldiphenylsilyl)-2,5-di-O-(4-methoxybenzyl)-D-mannitol
CAS No.:1421868-56-5
Molecular Formula:C₅₄H₆₆O₈Si₂
Molecular Weight:899.284
Hs Code.:
Mol file:1421868-56-5.mol

Synonyms:1,6-di-O-(tert-butyldiphenylsilyl)-2,5-di-O-(4-methoxybenzyl)-D-mannitol

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1,6-di-O-(tert-butyldiphenylsilyl)-2,5-di-O-(4-methoxybenzyl)-D-mannitol Edit

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Technology Process of 1,6-di-O-(tert-butyldiphenylsilyl)-2,5-di-O-(4-methoxybenzyl)-D-mannitol

There total 2 articles about 1,6-di-O-(tert-butyldiphenylsilyl)-2,5-di-O-(4-methoxybenzyl)-D-mannitol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

: 58479-61-1
tert-butylchlorodiphenylsilane

: 301298-48-6
2,5-di-O-(p-methoxybenzyl)-D-mannitol

: 1421868-56-5
1,6-di-O-(tert-butyldiphenylsilyl)-2,5-di-O-(4-methoxybenzyl)-D-mannitol

Guidance literature:: With 1H-imidazole; In N,N-dimethyl-formamide; at 0 - 20 ℃; regioselective reaction; Inert atmosphere;
DOI:10.1021/jo302508e

Reference yield:

: 1,3:4,6-di-O-benzylidene-2,5-bis-O-(p-methoxybenzyl)-D-mannitol

: 1421868-56-5
1,6-di-O-(tert-butyldiphenylsilyl)-2,5-di-O-(4-methoxybenzyl)-D-mannitol

Guidance literature:: Multi-step reaction with 2 steps

1: hydrogenchloride; water / methanol; hexane / 5 h / 20 °C

2: 1H-imidazole / N,N-dimethyl-formamide / 0 - 20 °C / Inert atmosphere

With 1H-imidazole; hydrogenchloride; water; In methanol; hexane; N,N-dimethyl-formamide;
DOI:10.1021/jo302508e