N,N'-bis<2-(2-methoxyanilino)-2,4,6-cycloheptatrienylidene>-1,5-pentanediamine

Base Information

Chemical Name:N,N'-bis<2-(2-methoxyanilino)-2,4,6-cycloheptatrienylidene>-1,5-pentanediamine
CAS No.:154177-91-0
Molecular Formula:C₃₃H₃₆N₄O₂
Molecular Weight:520.674
Hs Code.:

Synonyms:N,N'-bis<2-(2-methoxyanilino)-2,4,6-cycloheptatrienylidene>-1,5-pentanediamine

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N,N'-bis<2-(2-methoxyanilino)-2,4,6-cycloheptatrienylidene>-1,5-pentanediamine

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Technology Process of N,N'-bis<2-(2-methoxyanilino)-2,4,6-cycloheptatrienylidene>-1,5-pentanediamine

There total 4 articles about N,N'-bis<2-(2-methoxyanilino)-2,4,6-cycloheptatrienylidene>-1,5-pentanediamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 83.0%

: 462-94-2
1,5-diaminopentane

: 1-methoxy-2-(2-methoxyanilino)tropylium fluorosulfate

: 154177-91-0
N,N'-bis<2-(2-methoxyanilino)-2,4,6-cycloheptatrienylidene>-1,5-pentanediamine

Guidance literature:: With sodium carbonate; triethylamine; In methanol; for 24h; Ambient temperature;
DOI:10.1246/bcsj.66.2941

Reference yield: 82.0%

: 154177-90-9
N-<2-(2-methoxyanilino)-2,4,6-cycloheptatrienylidene>-1,5-pentanediamine

: 1-methoxy-2-(2-methoxyanilino)tropylium fluorosulfate

: 154177-91-0
N,N'-bis<2-(2-methoxyanilino)-2,4,6-cycloheptatrienylidene>-1,5-pentanediamine

Guidance literature:: With sodium carbonate; triethylamine; In methanol; for 24h; Ambient temperature;
DOI:10.1246/bcsj.66.2941

Reference yield:

: 67931-50-4
2-(2-methoxyanilino)tropone

: 154177-91-0
N,N'-bis<2-(2-methoxyanilino)-2,4,6-cycloheptatrienylidene>-1,5-pentanediamine

Guidance literature:: Multi-step reaction with 3 steps

1: 91 percent / CH₂Cl₂ / 24 h / Ambient temperature

2: 86 percent / Et₃N, Na₂CO₃ / methanol / 24 h / Ambient temperature

3: 82 percent / Et₃N, Na₂CO₃ / methanol / 24 h / Ambient temperature

With sodium carbonate; triethylamine; In methanol; dichloromethane;
DOI:10.1246/bcsj.66.2941