2-Phenyl-tetrahydro-pyrrolo[3,4-c]pyrrole-1,3-dione; compound with acetic acid

Base Information

Chemical Name:2-Phenyl-tetrahydro-pyrrolo[3,4-c]pyrrole-1,3-dione; compound with acetic acid
CAS No.:86732-44-7
Molecular Formula:C₂H₄O₂*C₁₂H₁₂N₂O₂
Molecular Weight:276.292
Hs Code.:

Synonyms:2-Phenyl-tetrahydro-pyrrolo[3,4-c]pyrrole-1,3-dione; compound with acetic acid

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Chemical Property of 2-Phenyl-tetrahydro-pyrrolo[3,4-c]pyrrole-1,3-dione; compound with acetic acid

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Technology Process of 2-Phenyl-tetrahydro-pyrrolo[3,4-c]pyrrole-1,3-dione; compound with acetic acid

There total 4 articles about 2-Phenyl-tetrahydro-pyrrolo[3,4-c]pyrrole-1,3-dione; compound with acetic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

: 86732-05-0
5-Benzyl-2-phenyl-5H-pyrrolo[3,4-c]pyrrole-1,3-dione

: 64-19-7,77671-22-8
acetic acid

: 86732-44-7
2-Phenyl-tetrahydro-pyrrolo[3,4-c]pyrrole-1,3-dione; compound with acetic acid

Guidance literature:: With hydrogen; palladium on activated charcoal; In acetic acid; at 55 ℃; for 18h; under 2585.7 Torr;

Reference yield:

: 86731-90-0
1-benzyl-pyrrole-3,4-dicarboxylic acid

: 86732-44-7
2-Phenyl-tetrahydro-pyrrolo[3,4-c]pyrrole-1,3-dione; compound with acetic acid

Guidance literature:: Multi-step reaction with 4 steps

1: 88 percent / dicyclohexylcarbodiimide / tetrahydrofuran / Heating; overnight

2: 93 percent / acetonitrile

3: 63 percent / SOCl₂ / dimethylformamide / 1 h / 50 - 60 °C

4: 91 percent / H₂ / 10percent Pd/C / acetic acid / 18 h / 55 °C / 2585.7 Torr

With thionyl chloride; hydrogen; dicyclohexyl-carbodiimide; palladium on activated charcoal; In tetrahydrofuran; acetic acid; N,N-dimethyl-formamide; acetonitrile;

Reference yield:

: 86731-92-2
1-benzyl-1H-pyrrole-3,4-dicarboxylic anhydride

: 86732-44-7
2-Phenyl-tetrahydro-pyrrolo[3,4-c]pyrrole-1,3-dione; compound with acetic acid

Guidance literature:: Multi-step reaction with 3 steps

1: 93 percent / acetonitrile

2: 63 percent / SOCl₂ / dimethylformamide / 1 h / 50 - 60 °C

3: 91 percent / H₂ / 10percent Pd/C / acetic acid / 18 h / 55 °C / 2585.7 Torr

With thionyl chloride; hydrogen; palladium on activated charcoal; In acetic acid; N,N-dimethyl-formamide; acetonitrile;