tris(triphenylphosphine)nickel(I) bromide

Base Information

Chemical Name:tris(triphenylphosphine)nickel(I) bromide
CAS No.:15245-43-9
Molecular Formula:C₅₄H₄₅BrNiP₃
Molecular Weight:925.467
Hs Code.:

Synonyms:tris(triphenylphosphine)nickel(I) bromide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of tris(triphenylphosphine)nickel(I) bromide

Chemical Property:

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Technology Process of tris(triphenylphosphine)nickel(I) bromide

There total 17 articles about tris(triphenylphosphine)nickel(I) bromide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

: 36673-36-6,111408-20-9,14126-37-5,54053-52-0
dibromobis(triphenylphosphine)nickel(II)

: 15245-43-9
tris(triphenylphosphine)nickel(I) bromide

Guidance literature:: With triphenylphosphine; zinc; In benzene; complex was treated with Zn dust; stirring for a few min; filtration into NiBr2(PPh3)2; filtration, concn., pptn. with MeOH, washing with MeOH, drying in vac.;elem. anal.;
DOI:10.1246/bcsj.53.2711

Reference yield: 61.0%

: 1295-35-8
bis(1,5-cyclooctadiene)nickel ⁽⁰⁾

: 2417-90-5
bromopropionitrile

: 15245-43-9
tris(triphenylphosphine)nickel(I) bromide

Guidance literature:: With P(C₆H₅)3; In toluene; (Ar); to a soln. of Ni(COD)2 and Ph3P Br(CH2)2CN is added; mixt. is kept. for 2 days at 5°C, ppt. is filtered off, washed with n-hexane and dried in vac., elem. anal.;

Reference yield: 58.0%

: 36673-36-6,111408-20-9,14126-37-5,54053-52-0
dibromobis(triphenylphosphine)nickel(II)

: 663627-53-0
[(o-C₆H₄PPh₂N(3,5-C₆H₃Me₂))Li]2*Et₂O

: 690634-63-0
[Ni(o-C₆H₄PPh₂N(3,5-C₆H₃Me₂))2]

: 15245-43-9
tris(triphenylphosphine)nickel(I) bromide

Guidance literature:: In tetrahydrofuran; (N2); a soln. of Li compd. and Ni complex dissolved in THF at -20°C, stirred at 25°C; elem. anal.;
DOI:10.1039/b305877h