2-[(E)-1-[1,1'-biphenyl]-4-yl-3-(4-methoxyphenyl)-4-methyl-4-nitropentylidene]-1-hydrazine carboxamide

Base Information

• Chemical Name: 2-[(E)-1-[1,1'-biphenyl]-4-yl-3-(4-methoxyphenyl)-4-methyl-4-nitropentylidene]-1-hydrazine carboxamide
• CAS No.: 878379-43-2
• Molecular Formula: C₂₆H₂₈N₄O₄
• Molecular Weight: 460.533

Synonyms:2-[(E)-1-[1,1'-biphenyl]-4-yl-3-(4-methoxyphenyl)-4-methyl-4-nitropentylidene]-1-hydrazine carboxamide

Chemical Property of 2-[(E)-1-[1,1'-biphenyl]-4-yl-3-(4-methoxyphenyl)-4-methyl-4-nitropentylidene]-1-hydrazine carboxamide

Chemical Property:

Purity/Quality:

98% ^*data from raw suppliers

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Technology Process of 2-[(E)-1-[1,1'-biphenyl]-4-yl-3-(4-methoxyphenyl)-4-methyl-4-nitropentylidene]-1-hydrazine carboxamide

There total 2 articles about 2-[(E)-1-[1,1'-biphenyl]-4-yl-3-(4-methoxyphenyl)-4-methyl-4-nitropentylidene]-1-hydrazine carboxamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 43.0%

1-[1,1'-biphenyl]-4-yl-3-(4-methoxyphenyl)-4-methyl-4-nitro-1-pentanone (878379-59-0) + semicarbazide hydrochloride (563-41-7) → 2-[(E)-1-[1,1'-biphenyl]-4-yl-3-(4-methoxyphenyl)-4-methyl-4-nitropentylidene]-1-hydrazine carboxamide (878379-43-2)

Guidance literature:

With sodium acetate; In ethanol; for 4h; Heating;

DOI:10.1002/jhet.5570430122

Reference yield:

(E)-1-([1,1'-biphenyl]-4-yl)-3-(4-methoxyphenyl)prop-2-en-1-one (102692-38-6) → 2-[(E)-1-[1,1'-biphenyl]-4-yl-3-(4-methoxyphenyl)-4-methyl-4-nitropentylidene]-1-hydrazine carboxamide (878379-43-2)

Guidance literature:

Multi-step reaction with 2 steps

1: sodium ethoxide / ethanol / 5 h / Heating

2: 43 percent / aq. sodium acetate / ethanol / 4 h / Heating

With sodium ethanolate; sodium acetate; In ethanol;

DOI:10.1002/jhet.5570430122

Reference yield: 66.0%

2-[(E)-1-[1,1'-biphenyl]-4-yl-3-(4-methoxyphenyl)-4-methyl-4-nitropentylidene]-1-hydrazine carboxamide (878379-43-2) → 4-[1,1'-biphenyl]-4-yl-5-[1-(4-methoxyphenyl)-2-methyl-2-nitropropyl]-1,2,3-selenadiazole

Guidance literature:

With selenium(IV) oxide; In tetrahydrofuran; for 2h; Heating;

DOI:10.1002/jhet.5570430122

upstream raw materials:

1-[1,1'-biphenyl]-4-yl-3-(4-methoxyphenyl)-4-methyl-4-nitro-1-pentanone

semicarbazide hydrochloride

(E)-1-([1,1'-biphenyl]-4-yl)-3-(4-methoxyphenyl)prop-2-en-1-one

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