Methanesulfonic acid 6-(benzyloxycarbonyl-propyl-amino)-1-ethyl-hexyl ester

Base Information

Chemical Name:Methanesulfonic acid 6-(benzyloxycarbonyl-propyl-amino)-1-ethyl-hexyl ester
CAS No.:120476-72-4
Molecular Formula:C₂₀H₃₃NO₅S
Molecular Weight:399.552
Hs Code.:

Synonyms:Methanesulfonic acid 6-(benzyloxycarbonyl-propyl-amino)-1-ethyl-hexyl ester

Suppliers and Price of Methanesulfonic acid 6-(benzyloxycarbonyl-propyl-amino)-1-ethyl-hexyl ester

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of Methanesulfonic acid 6-(benzyloxycarbonyl-propyl-amino)-1-ethyl-hexyl ester

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of Methanesulfonic acid 6-(benzyloxycarbonyl-propyl-amino)-1-ethyl-hexyl ester

There total 4 articles about Methanesulfonic acid 6-(benzyloxycarbonyl-propyl-amino)-1-ethyl-hexyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 64.0%

: 124-63-0
methanesulfonyl chloride

: 120476-57-5
N-(carbobenzyloxy)-N-propyl-6-hydroxyoctylamine

: 120476-72-4
Methanesulfonic acid 6-(benzyloxycarbonyl-propyl-amino)-1-ethyl-hexyl ester

Guidance literature:: With triethylamine; In dichloromethane; Ambient temperature;
DOI:10.1021/jm00126a026

Reference yield:

: 29094-05-1
6-ethyl-ε-caprolactone

: 120476-72-4
Methanesulfonic acid 6-(benzyloxycarbonyl-propyl-amino)-1-ethyl-hexyl ester

Guidance literature:: Multi-step reaction with 4 steps

1: 70 percent / (CH₃)3Al / benzene; hexane / 4 h / Heating

2: B₂H₆*THF / a) reflux, 2 h, b) r.t., overnight

3: 75 percent / 1M KOH / diethyl ether / Ambient temperature

4: 64 percent / Et₃N / CH₂Cl₂ / Ambient temperature

With potassium hydroxide; B₂H₆-THF; trimethylaluminum; triethylamine; In diethyl ether; hexane; dichloromethane; benzene;
DOI:10.1021/jm00126a026

Reference yield:

: 120476-55-3
N-propyl-6-hydroxyoctylamine

: 120476-72-4
Methanesulfonic acid 6-(benzyloxycarbonyl-propyl-amino)-1-ethyl-hexyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 75 percent / 1M KOH / diethyl ether / Ambient temperature

2: 64 percent / Et₃N / CH₂Cl₂ / Ambient temperature

With potassium hydroxide; triethylamine; In diethyl ether; dichloromethane;
DOI:10.1021/jm00126a026