4-amino-2-<(diethylamino)methyl>-6-(1-methylethyl)phenol dihydrochloride

Base Information

Chemical Name:4-amino-2-<(diethylamino)methyl>-6-(1-methylethyl)phenol dihydrochloride
CAS No.:107244-72-4
Molecular Formula:C₁₄H₂₄N₂O*2ClH
Molecular Weight:309.279
Hs Code.:

Synonyms:4-amino-2-<(diethylamino)methyl>-6-(1-methylethyl)phenol dihydrochloride

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Chemical Property of 4-amino-2-<(diethylamino)methyl>-6-(1-methylethyl)phenol dihydrochloride

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Technology Process of 4-amino-2-<(diethylamino)methyl>-6-(1-methylethyl)phenol dihydrochloride

There total 5 articles about 4-amino-2-<(diethylamino)methyl>-6-(1-methylethyl)phenol dihydrochloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 88-69-7
2-(1-methylethyl)phenol

: 107244-72-4
4-amino-2-<(diethylamino)methyl>-6-(1-methylethyl)phenol dihydrochloride

Guidance literature:: Multi-step reaction with 5 steps

1: 34 percent / aq. HCl, NaNO₂ / aq. ethanol / 5 h / 0 °C

2: H₂ / Ni (Ra) / methanol / 5.5 h / 2663.3 Torr

3: methanol; tetrahydrofuran / 0.5 h / Heating

4: 87 percent / ethanol / 48 h / Heating

5: 6N aq. HCl / 1 h / Heating

With hydrogenchloride; hydrogen; sodium nitrite; nickel; In tetrahydrofuran; methanol; ethanol;
DOI:10.1021/jm00388a027

Reference yield:

: 107244-57-5
2-isopropyl-[1,4]benzoquinone 4-oxime

: 107244-72-4
4-amino-2-<(diethylamino)methyl>-6-(1-methylethyl)phenol dihydrochloride

Guidance literature:: Multi-step reaction with 4 steps

1: H₂ / Ni (Ra) / methanol / 5.5 h / 2663.3 Torr

2: methanol; tetrahydrofuran / 0.5 h / Heating

3: 87 percent / ethanol / 48 h / Heating

4: 6N aq. HCl / 1 h / Heating

With hydrogenchloride; hydrogen; nickel; In tetrahydrofuran; methanol; ethanol;
DOI:10.1021/jm00388a027

Reference yield:

: 16750-66-6
2-iso-Propyl-4-aminophenol

: 107244-72-4
4-amino-2-<(diethylamino)methyl>-6-(1-methylethyl)phenol dihydrochloride

Guidance literature:: Multi-step reaction with 3 steps

1: methanol; tetrahydrofuran / 0.5 h / Heating

2: 87 percent / ethanol / 48 h / Heating

3: 6N aq. HCl / 1 h / Heating

With hydrogenchloride; In tetrahydrofuran; methanol; ethanol;
DOI:10.1021/jm00388a027