1-[2-(N,N-dimethylamino)phenyl]-2-methoxynaphthalene

Base Information

Chemical Name:1-[2-(N,N-dimethylamino)phenyl]-2-methoxynaphthalene
CAS No.:544428-91-3
Molecular Formula:C₁₉H₁₉NO
Molecular Weight:277.366
Hs Code.:

Synonyms:1-[2-(N,N-dimethylamino)phenyl]-2-methoxynaphthalene

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Chemical Property of 1-[2-(N,N-dimethylamino)phenyl]-2-methoxynaphthalene

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Technology Process of 1-[2-(N,N-dimethylamino)phenyl]-2-methoxynaphthalene

There total 1 articles about 1-[2-(N,N-dimethylamino)phenyl]-2-methoxynaphthalene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

: 721929-72-2
(+/-)-2-(2'-methoxynaphthalen-1-yl)phenylamine

: 74-88-4
methyl iodide

: 544428-91-3
1-[2-(N,N-dimethylamino)phenyl]-2-methoxynaphthalene

Guidance literature:: With potassium hydrogencarbonate; In N,N-dimethyl-formamide; at 20 ℃; for 4h; Inert atmosphere;
DOI:10.1021/ol102539x

Reference yield: 89.0%

: 544428-91-3
1-[2-(N,N-dimethylamino)phenyl]-2-methoxynaphthalene

: 1258452-99-1
1-[2-(N,N-dimethylamino)phenyl]-2-hydroxynaphthalene

Guidance literature:: 1-[2-(N,N-dimethylamino)phenyl]-2-methoxynaphthalene; With boron tribromide; In dichloromethane; at 20 ℃; for 9h; Inert atmosphere; Cooling with ice;

With water; sodium hydroxide; In dichloromethane; pH=7;
DOI:10.1021/ol102539x

Reference yield:

: 544428-91-3
1-[2-(N,N-dimethylamino)phenyl]-2-methoxynaphthalene

: 1258453-00-7
2-(2-hydroxy-1-naphthyl)phenyltrimethylammonium iodide

Guidance literature:: Multi-step reaction with 2 steps

1.1: boron tribromide / dichloromethane / 9 h / 20 °C / Inert atmosphere; Cooling with ice

1.2: pH 7

2.1: N,N-dimethyl-formamide / 72 h / 40 °C / Inert atmosphere

With boron tribromide; In dichloromethane; N,N-dimethyl-formamide;
DOI:10.1021/ol102539x