(Z)-3-((2S,3R)-4-Oxo-3-phenylacetylamino-azetidin-2-ylsulfanyl)-acrylic acid methyl ester

Base Information

Chemical Name:(Z)-3-((2S,3R)-4-Oxo-3-phenylacetylamino-azetidin-2-ylsulfanyl)-acrylic acid methyl ester
CAS No.:104486-78-4
Molecular Formula:C₁₅H₁₆N₂O₄S
Molecular Weight:320.369
Hs Code.:

Synonyms:(Z)-3-((2S,3R)-4-Oxo-3-phenylacetylamino-azetidin-2-ylsulfanyl)-acrylic acid methyl ester

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (Z)-3-((2S,3R)-4-Oxo-3-phenylacetylamino-azetidin-2-ylsulfanyl)-acrylic acid methyl ester

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Technology Process of (Z)-3-((2S,3R)-4-Oxo-3-phenylacetylamino-azetidin-2-ylsulfanyl)-acrylic acid methyl ester

There total 1 articles about (Z)-3-((2S,3R)-4-Oxo-3-phenylacetylamino-azetidin-2-ylsulfanyl)-acrylic acid methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 35.0%

: 74213-36-8,74243-81-5,104486-77-3
(1S,5R)-3-benzyl-6-(2-bromo-1-hydroxy-2-methylpropyl)-4-oxa-2,6-diazabicyclo<3.2.0>hept-2-en-7-one

: 69077-84-5
cis-β-(methoxycarbonyl)vinylisothiouronium chloride

: 104486-78-4
(Z)-3-((2S,3R)-4-Oxo-3-phenylacetylamino-azetidin-2-ylsulfanyl)-acrylic acid methyl ester

: 104430-41-3
(Z)-3-((2R,3R)-4-Oxo-3-phenylacetylamino-azetidin-2-ylsulfanyl)-acrylic acid methyl ester

Guidance literature:: With triethylamine; Yield given. Multistep reaction; 1.) dichloromethane;
DOI:10.1016/S0040-4039(00)84243-4

Reference yield:

: 7633-32-1
tert-butyl glyoxylate

: 104486-78-4
(Z)-3-((2S,3R)-4-Oxo-3-phenylacetylamino-azetidin-2-ylsulfanyl)-acrylic acid methyl ester

: 104430-43-5
(4S,6S,7R)-4-Methoxycarbonylmethyl-8-oxo-7-phenylacetylamino-3,5-dithia-1-aza-bicyclo[4.2.0]octane-2-carboxylic acid tert-butyl ester

Guidance literature:: With 2,6-dimethylpyridine; thionyl chloride; hydrogen sulfide; triethylamine; Yield given. Multistep reaction;
DOI:10.1016/S0040-4039(00)84243-4