C₄₃H₅₅N₃O₄

Base Information

Chemical Name:C₄₃H₅₅N₃O₄
CAS No.:1280736-99-3
Molecular Formula:C₄₃H₅₅N₃O₄
Molecular Weight:677.927
Hs Code.:

C<sub>43</sub>H<sub>55</sub>N<sub>3</sub>O<sub>4</sub>

Synonyms:C₄₃H₅₅N₃O₄

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Chemical Property of C₄₃H₅₅N₃O₄

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Technology Process of C₄₃H₅₅N₃O₄

There total 8 articles about C₄₃H₅₅N₃O₄ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.0%

: 1280736-93-7
C₅₁H₆₁N₃O₆

: 1280736-99-3
C₄₃H₅₅N₃O₄

Guidance literature:: With 20 % Pd(OH)2/C; hydrogen; In methanol; at 20 ℃; for 16h; under 3800.26 Torr; chemoselective reaction;
DOI:10.1016/j.tetasy.2010.12.007

Reference yield:

: 820236-49-5
tert-butyl (1S,2S,3S,αS)-3-benzyl-2-(N-benzyl-N-α-methylbenzylamino)-cyclopentane-1-carboxylate

: 1280736-99-3
C₄₃H₅₅N₃O₄

Guidance literature:: Multi-step reaction with 7 steps

1: 20 % Pd(OH)2/C; hydrogen / ethyl acetate / 16 h / 20 °C / 3800.26 Torr

2: triethylamine / tetrahydrofuran / 16 h / 0 - 20 °C / Inert atmosphere

3: trifluoroacetic acid / dichloromethane / 3 h / 0 - 20 °C / Inert atmosphere

4: benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine / chloroform / 16 h / 20 °C / Inert atmosphere

5: 20 % Pd(OH)2/C; hydrogen / methanol / 16 h / 20 °C / 3800.26 Torr

6: benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine / chloroform / 16 h / 20 °C / Inert atmosphere

7: 20 % Pd(OH)2/C; hydrogen / methanol / 16 h / 20 °C / 3800.26 Torr

With 20 % Pd(OH)2/C; hydrogen; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; trifluoroacetic acid; In tetrahydrofuran; methanol; dichloromethane; chloroform; ethyl acetate;
DOI:10.1016/j.tetasy.2010.12.007

Reference yield:

: 816444-33-4
tert-butyl (1R,2S,3S,αS)-3-benzyl-2-(N-benzyl-N-α-methylbenzylamino)-cyclopentane-1-carboxylate

: 1280736-99-3
C₄₃H₅₅N₃O₄

Guidance literature:: Multi-step reaction with 8 steps

1: potassium tert-butylate; tert-butyl alcohol / 8 h / Reflux; Inert atmosphere

2: 20 % Pd(OH)2/C; hydrogen / ethyl acetate / 16 h / 20 °C / 3800.26 Torr

3: triethylamine / tetrahydrofuran / 16 h / 0 - 20 °C / Inert atmosphere

4: trifluoroacetic acid / dichloromethane / 3 h / 0 - 20 °C / Inert atmosphere

5: benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine / chloroform / 16 h / 20 °C / Inert atmosphere

6: 20 % Pd(OH)2/C; hydrogen / methanol / 16 h / 20 °C / 3800.26 Torr

7: benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine / chloroform / 16 h / 20 °C / Inert atmosphere

8: 20 % Pd(OH)2/C; hydrogen / methanol / 16 h / 20 °C / 3800.26 Torr

With 20 % Pd(OH)2/C; potassium tert-butylate; hydrogen; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; trifluoroacetic acid; tert-butyl alcohol; In tetrahydrofuran; methanol; dichloromethane; chloroform; ethyl acetate;
DOI:10.1016/j.tetasy.2010.12.007