p-methoxyphenyl 2,3,6-tri-O-benzoyl-4-O-levulinoyl-β-D-galactopyranoside

Base Information

Chemical Name:p-methoxyphenyl 2,3,6-tri-O-benzoyl-4-O-levulinoyl-β-D-galactopyranoside
CAS No.:933045-19-3
Molecular Formula:C₃₉H₃₆O₁₂
Molecular Weight:696.708
Hs Code.:

Synonyms:p-methoxyphenyl 2,3,6-tri-O-benzoyl-4-O-levulinoyl-β-D-galactopyranoside

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of p-methoxyphenyl 2,3,6-tri-O-benzoyl-4-O-levulinoyl-β-D-galactopyranoside

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Technology Process of p-methoxyphenyl 2,3,6-tri-O-benzoyl-4-O-levulinoyl-β-D-galactopyranoside

There total 1 articles about p-methoxyphenyl 2,3,6-tri-O-benzoyl-4-O-levulinoyl-β-D-galactopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.0%

: 123-76-2
levulinic acid

: 312957-72-5
4-methoxyphenyl 2,3,6-tri-O-benzoyl-β-D-galactopyranoside

: 933045-19-3
p-methoxyphenyl 2,3,6-tri-O-benzoyl-4-O-levulinoyl-β-D-galactopyranoside

Guidance literature:: With dmap; dicyclohexyl-carbodiimide; In dichloromethane; at 0 - 20 ℃; for 15h;
DOI:10.1016/j.tet.2007.01.011

Reference yield:

: 933045-19-3
p-methoxyphenyl 2,3,6-tri-O-benzoyl-4-O-levulinoyl-β-D-galactopyranoside

: 2,3,6-tri-O-benzoyl-4-O-levulinoyl-D-galactopyranose

Guidance literature:: With ammonium cerium(IV) nitrate; In water; toluene; acetonitrile; at 0 - 20 ℃; for 4.5h;
DOI:10.1016/j.tet.2007.01.011

Reference yield:

: 933045-19-3
p-methoxyphenyl 2,3,6-tri-O-benzoyl-4-O-levulinoyl-β-D-galactopyranoside

: 195323-29-6
2,3,6-tri-O-benzoyl-4-O-levulinoyl-α-D-galactopyranosyl 2,2,2-trichloroacetimidate

Guidance literature:: Multi-step reaction with 2 steps

1: cerium(IV) ammonium nitrate / toluene; acetonitrile; H₂O / 4.5 h / 0 - 20 °C

2: 1.35 g / DBU / CH₂Cl₂ / 1.5 h / 20 °C

With ammonium cerium(IV) nitrate; 1,8-diazabicyclo[5.4.0]undec-7-ene; In dichloromethane; water; toluene; acetonitrile;
DOI:10.1016/j.tet.2007.01.011