N¹-(p-Chlorobenzoyl)-N¹-(p-methylphenyl)-N²-(m-nitrophenyl)-acetamidine

Base Information

Chemical Name:N¹-(p-Chlorobenzoyl)-N¹-(p-methylphenyl)-N²-(m-nitrophenyl)-acetamidine
CAS No.:130118-00-2
Molecular Formula:C₂₂H₁₈ClN₃O₃
Molecular Weight:407.856
Hs Code.:

N<sup>1</sup>-(p-Chlorobenzoyl)-N<sup>1</sup>-(p-methylphenyl)-N<sup>2</sup>-(m-nitrophenyl)-acetamidine

Synonyms:N¹-(p-Chlorobenzoyl)-N¹-(p-methylphenyl)-N²-(m-nitrophenyl)-acetamidine

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Chemical Property of N¹-(p-Chlorobenzoyl)-N¹-(p-methylphenyl)-N²-(m-nitrophenyl)-acetamidine

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Technology Process of N¹-(p-Chlorobenzoyl)-N¹-(p-methylphenyl)-N²-(m-nitrophenyl)-acetamidine

There total 3 articles about N¹-(p-Chlorobenzoyl)-N¹-(p-methylphenyl)-N²-(m-nitrophenyl)-acetamidine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 37.0%

: 2447-95-2
4-chloro-N-(4-tolyl)benzamide

: 130117-85-0
N¹-Tosyl-N¹-(p-nitrophenyl)-N²-(m-nitrophenyl)acetamidine

: 130118-00-2
N¹-(p-Chlorobenzoyl)-N¹-(p-methylphenyl)-N²-(m-nitrophenyl)-acetamidine

Guidance literature:: With potassium tert-butylate; In tetrahydrofuran; for 24h; Ambient temperature;
DOI:10.1248/cpb.38.1379

Reference yield:

: 130117-96-3
m-Nitroacetophenonoxime tosylate

: 130118-00-2
N¹-(p-Chlorobenzoyl)-N¹-(p-methylphenyl)-N²-(m-nitrophenyl)-acetamidine

Guidance literature:: Multi-step reaction with 2 steps

1: 39 percent / dimethylformamide / 2 h / 90 °C

2: 37 percent / tert-BuOK / tetrahydrofuran / 24 h / Ambient temperature

With potassium tert-butylate; In tetrahydrofuran; N,N-dimethyl-formamide;
DOI:10.1248/cpb.38.1379

Reference yield:

: 87974-55-8
(E)-1-(3-nitrophenyl)ethan-1-one oxime

: 130118-00-2
N¹-(p-Chlorobenzoyl)-N¹-(p-methylphenyl)-N²-(m-nitrophenyl)-acetamidine

Guidance literature:: Multi-step reaction with 3 steps

1: 69 percent / Et₃N / benzene / 24 h / Ambient temperature

2: 39 percent / dimethylformamide / 2 h / 90 °C

3: 37 percent / tert-BuOK / tetrahydrofuran / 24 h / Ambient temperature

With potassium tert-butylate; triethylamine; In tetrahydrofuran; N,N-dimethyl-formamide; benzene;
DOI:10.1248/cpb.38.1379