N₁-[(5''-acetoxyethoxy)methyl]-5'-O-TBDPS-2',3'-O-isopropylidene-8-tifluoromethylinosine

Base Information

• Chemical Name: N₁-[(5''-acetoxyethoxy)methyl]-5'-O-TBDPS-2',3'-O-isopropylidene-8-tifluoromethylinosine
• CAS No.: 1256503-24-8
• Molecular Formula: C₃₅H₄₁F₃N₄O₈Si
• Molecular Weight: 730.813

Synonyms:N₁-[(5''-acetoxyethoxy)methyl]-5'-O-TBDPS-2',3'-O-isopropylidene-8-tifluoromethylinosine

Chemical Property of N₁-[(5''-acetoxyethoxy)methyl]-5'-O-TBDPS-2',3'-O-isopropylidene-8-tifluoromethylinosine

Chemical Property:

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Technology Process of N₁-[(5''-acetoxyethoxy)methyl]-5'-O-TBDPS-2',3'-O-isopropylidene-8-tifluoromethylinosine

There total 1 articles about N₁-[(5''-acetoxyethoxy)methyl]-5'-O-TBDPS-2',3'-O-isopropylidene-8-tifluoromethylinosine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 59.0%

2,2-difluoro-2-(fluorosulfonyl)acetate (680-15-9) + N1-[(5''-acetoxyethoxy)methyl]-5'-O-TBDPS-2',3'-O-isopropylidene-8-bromoinosine (1256503-23-7) → N1-[(5''-acetoxyethoxy)methyl]-5'-O-TBDPS-2',3'-O-isopropylidene-8-tifluoromethylinosine (1256503-24-8)

Guidance literature:

With N,N,N,N,N,N-hexamethylphosphoric triamide; copper(l) iodide; In N,N-dimethyl-formamide; at 70 ℃; for 12h; Inert atmosphere;

DOI:10.1039/c0ob00090f

upstream raw materials:

2,2-difluoro-2-(fluorosulfonyl)acetate

N₁-[(5''-acetoxyethoxy)methyl]-5'-O-TBDPS-2',3'-O-isopropylidene-8-bromoinosine

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