9,10-Dibutoxyanthracene

Base Information

• Chemical Name: 9,10-Dibutoxyanthracene
• CAS No.: 76275-14-4
• Molecular Formula: C₂₂H₂₆O₂
• Molecular Weight: 322.447
• Hs Code.: 29093090
• Mol file: 76275-14-4.mol

Synonyms:Anthracure UVS 1331;DBA (sensitizer);UVS 1331;

Chemical Property of 9,10-Dibutoxyanthracene

Chemical Property:

• Boiling Point: 478.84 °C at 760 mmHg
• Flash Point: 179.209 °C
• PSA: 18.46000
• Density: 1.058 g/cm³
• LogP: 6.35080
• Storage Temp.: Sealed in dry,Room Temperature

Purity/Quality:

99% ^*data from raw suppliers

9,10-Dibutoxyanthracene 98% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 9,10-Dibutoxyanthracene

There total 4 articles about 9,10-Dibutoxyanthracene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.0%

n-Butyl chloride (109-69-3) + 9,10-phenanthrenequinone (84-65-1) → 9,10-dibutoxyanthracene (76275-14-4)

Guidance literature:

With tetrabutylammomium bromide; iron; sodium hydroxide; zinc; In water; toluene; at 50 - 65 ℃; for 2h;

Reference yield: 96.0%

1-bromo-butane (109-65-9) + 9,10-phenanthrenequinone (84-65-1) → 9,10-dibutoxyanthracene (76275-14-4)

Guidance literature:

With tetrabutylammomium bromide; iron; sodium hydroxide; zinc; In water; toluene; at 50 - 65 ℃; for 2h; Reagent/catalyst; Temperature;

Reference yield: 70.0%

1-bromo-butane (109-65-9) + 9,10-dihydroxyanthracene disodium salt (46492-07-3) → 9,10-dibutoxyanthracene (76275-14-4)

Guidance literature:

In DMF (N,N-dimethyl-formamide); water; at 65 - 70 ℃; for 2h; Product distribution / selectivity;

upstream raw materials:

1-bromo-butane

9,10-phenanthrenequinone

9,10-dihydroxyanthracene disodium salt

n-Butyl chloride

Refernces

• 1、 -. "PROCESS FOR PRODUCING ANTHRACENE DIETHER". Page/Page column 9. . Retrieved 2008/06/13.