4-Oxo-2,6,8-triphenyl-3,4-dihydropyrido<2,1-f><1,2,4>triazin-9-ium-3-olate

Base Information

• Chemical Name: 4-Oxo-2,6,8-triphenyl-3,4-dihydropyrido<2,1-f><1,2,4>triazin-9-ium-3-olate
• CAS No.: 106366-97-6
• Molecular Formula: C₂₅H₁₇N₃O₂
• Molecular Weight: 391.429

Synonyms:4-Oxo-2,6,8-triphenyl-3,4-dihydropyrido<2,1-f><1,2,4>triazin-9-ium-3-olate

Chemical Property of 4-Oxo-2,6,8-triphenyl-3,4-dihydropyrido<2,1-f><1,2,4>triazin-9-ium-3-olate

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
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Technology Process of 4-Oxo-2,6,8-triphenyl-3,4-dihydropyrido<2,1-f><1,2,4>triazin-9-ium-3-olate

There total 3 articles about 4-Oxo-2,6,8-triphenyl-3,4-dihydropyrido<2,1-f><1,2,4>triazin-9-ium-3-olate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 78.0%

N-Benzamido-2-ethoxycarbonyl-4,6-diphenylpyridinium tetrafluoroborate → 4-Oxo-2,6,8-triphenyl-3,4-dihydropyrido<2,1-f><1,2,4>triazin-9-ium-3-olate (106366-97-6)

Guidance literature:

With hydroxylamine hydrochloride; In ethanol; for 8h; Heating;

DOI:10.1055/s-1986-31629

Reference yield:

2-(ethoxycarbonyl)-4,6-diphenylpyrylium tetrafluoroborate → 4-Oxo-2,6,8-triphenyl-3,4-dihydropyrido<2,1-f><1,2,4>triazin-9-ium-3-olate (106366-97-6)

Guidance literature:

Multi-step reaction with 2 steps

1: 86 percent / ethanol / 18 h / Ambient temperature

2: 78 percent / hydroxylamine hydrochloride / aq. ethanol / 8 h / Heating

With hydroxylamine hydrochloride; In ethanol;

DOI:10.1055/s-1986-31629

Reference yield:

benzoic acid hydrazide (613-94-5) → 4-Oxo-2,6,8-triphenyl-3,4-dihydropyrido<2,1-f><1,2,4>triazin-9-ium-3-olate (106366-97-6)

Guidance literature:

Multi-step reaction with 2 steps

1: 86 percent / ethanol / 18 h / Ambient temperature

2: 78 percent / hydroxylamine hydrochloride / aq. ethanol / 8 h / Heating

With hydroxylamine hydrochloride; In ethanol;

DOI:10.1055/s-1986-31629

upstream raw materials:

benzoic acid hydrazide

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