N-(3-{4-[2-(dimethylamino)ethoxy]phenyl}propyl)-4,5-dimethyl-2-nitroaniline

Base Information

Chemical Name:N-(3-{4-[2-(dimethylamino)ethoxy]phenyl}propyl)-4,5-dimethyl-2-nitroaniline
CAS No.:1338684-54-0
Molecular Formula:C₂₁H₂₉N₃O₃
Molecular Weight:371.48
Hs Code.:

Synonyms:N-(3-{4-[2-(dimethylamino)ethoxy]phenyl}propyl)-4,5-dimethyl-2-nitroaniline

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Chemical Property of N-(3-{4-[2-(dimethylamino)ethoxy]phenyl}propyl)-4,5-dimethyl-2-nitroaniline

Chemical Property:

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Technology Process of N-(3-{4-[2-(dimethylamino)ethoxy]phenyl}propyl)-4,5-dimethyl-2-nitroaniline

There total 4 articles about N-(3-{4-[2-(dimethylamino)ethoxy]phenyl}propyl)-4,5-dimethyl-2-nitroaniline which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 38.0%

: 1338684-53-9
N-(3-{4-[2-(dimethylamino)ethoxy]phenyl}propyl)-N-(4,5-dimethyl-2-nitrophenyl)-2,2,2-trifluoroacetamide

: 1338684-54-0
N-(3-{4-[2-(dimethylamino)ethoxy]phenyl}propyl)-4,5-dimethyl-2-nitroaniline

Guidance literature:: With potassium carbonate; In methanol; at 20 ℃; for 18h;

Reference yield:

: 5597-50-2
3-(4-hydroxyphenyl)propionic acid methyl ester

: 1338684-54-0
N-(3-{4-[2-(dimethylamino)ethoxy]phenyl}propyl)-4,5-dimethyl-2-nitroaniline

Guidance literature:: Multi-step reaction with 4 steps

1: triphenylphosphine; di-isopropyl azodicarboxylate / tetrahydrofuran / 18 h / 20 °C

2: lithium borohydride / tetrahydrofuran / 18 h / 20 °C

3: triphenylphosphine; di-isopropyl azodicarboxylate / 1,2-dimethoxyethane / 0 - 20 °C

4: potassium carbonate / methanol / 18 h / 20 °C

With lithium borohydride; di-isopropyl azodicarboxylate; potassium carbonate; triphenylphosphine; In tetrahydrofuran; methanol; 1,2-dimethoxyethane;

Reference yield:

: 1338684-51-7
methyl 3-{4-[2-(dimethylamino)ethoxy]phenyl}propanoate

: 1338684-54-0
N-(3-{4-[2-(dimethylamino)ethoxy]phenyl}propyl)-4,5-dimethyl-2-nitroaniline

Guidance literature:: Multi-step reaction with 3 steps

1: lithium borohydride / tetrahydrofuran / 18 h / 20 °C

2: triphenylphosphine; di-isopropyl azodicarboxylate / 1,2-dimethoxyethane / 0 - 20 °C

3: potassium carbonate / methanol / 18 h / 20 °C

With lithium borohydride; di-isopropyl azodicarboxylate; potassium carbonate; triphenylphosphine; In tetrahydrofuran; methanol; 1,2-dimethoxyethane;